(1R,2R)-2-(3,5-dinitrobenzamido)cyclohexyl bis(2-methoxybenzyl)carbamodithioate

Base Information

Chemical Name:(1R,2R)-2-(3,5-dinitrobenzamido)cyclohexyl bis(2-methoxybenzyl)carbamodithioate
CAS No.:1292810-13-9
Molecular Formula:C₃₀H₃₂N₄O₇S₂
Molecular Weight:624.739
Hs Code.:

Synonyms:(1R,2R)-2-(3,5-dinitrobenzamido)cyclohexyl bis(2-methoxybenzyl)carbamodithioate

Suppliers and Price of (1R,2R)-2-(3,5-dinitrobenzamido)cyclohexyl bis(2-methoxybenzyl)carbamodithioate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (1R,2R)-2-(3,5-dinitrobenzamido)cyclohexyl bis(2-methoxybenzyl)carbamodithioate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (1R,2R)-2-(3,5-dinitrobenzamido)cyclohexyl bis(2-methoxybenzyl)carbamodithioate

There total 1 articles about (1R,2R)-2-(3,5-dinitrobenzamido)cyclohexyl bis(2-methoxybenzyl)carbamodithioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75-15-0,12122-00-8
carbon disulfide

: 884588-09-4
7-(3,5-dinitrobenzoyl)-7-azabicyclo[4.1.0]heptane

: 178903-65-6
bis(2-methoxybenzyl)amine

: 1292810-13-9
(1R,2R)-2-(3,5-dinitrobenzamido)cyclohexyl bis(2-methoxybenzyl)carbamodithioate

: (1S,2S)-2-(3,5-dinitrobenzamido)cyclohexyl bis(2-methoxybenzyl)carbamodithioate

Guidance literature:: carbon disulfide; 7-(3,5-dinitrobenzoyl)-7-azabicyclo[4.1.0]heptane; With (1R,2R)-2-(tert-butyldiphenylsilyloxy)-N-(dipyrrolidin-1-ylmethylene)-2,3-dihydro-1H-inden-1-amine; In diethyl ether; at -50 ℃; for 0.5h; Inert atmosphere;

bis(2-methoxybenzyl)amine; In diethyl ether; at -50 ℃; for 24h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1039/c0cc05840h

Reference yield: 78.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 1292810-13-9
(1R,2R)-2-(3,5-dinitrobenzamido)cyclohexyl bis(2-methoxybenzyl)carbamodithioate

: 1292810-21-9
(1R,2R)-2-(bis(2-methoxybenzyl)carbamothioylthio)cyclohexylcarbamate

Guidance literature:: di-tert-butyl dicarbonate; (1R,2R)-2-(3,5-dinitrobenzamido)cyclohexyl bis(2-methoxybenzyl)carbamodithioate; With dmap; triethylamine; In tetrahydrofuran; at 20 ℃; for 48h; Inert atmosphere;

With sodium hydroxide; In tetrahydrofuran; water; at 20 ℃; for 2h;
DOI:10.1039/c0cc05840h