(1R,2R)-2-(bis(2-methoxybenzyl)carbamothioylthio)cyclohexylcarbamate

Base Information

• Chemical Name: (1R,2R)-2-(bis(2-methoxybenzyl)carbamothioylthio)cyclohexylcarbamate
• CAS No.: 1292810-21-9
• Molecular Formula: C₂₈H₃₈N₂O₄S₂
• Molecular Weight: 530.753
• Mol file: 1292810-21-9.mol

Synonyms:(1R,2R)-2-(bis(2-methoxybenzyl)carbamothioylthio)cyclohexylcarbamate

Chemical Property of (1R,2R)-2-(bis(2-methoxybenzyl)carbamothioylthio)cyclohexylcarbamate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (1R,2R)-2-(bis(2-methoxybenzyl)carbamothioylthio)cyclohexylcarbamate

There total 1 articles about (1R,2R)-2-(bis(2-methoxybenzyl)carbamothioylthio)cyclohexylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

di-tert-butyl dicarbonate (24424-99-5) + (1R,2R)-2-(3,5-dinitrobenzamido)cyclohexyl bis(2-methoxybenzyl)carbamodithioate (1292810-13-9) → (1R,2R)-2-(bis(2-methoxybenzyl)carbamothioylthio)cyclohexylcarbamate (1292810-21-9)

Guidance literature:

di-tert-butyl dicarbonate; (1R,2R)-2-(3,5-dinitrobenzamido)cyclohexyl bis(2-methoxybenzyl)carbamodithioate; With dmap; triethylamine; In tetrahydrofuran; at 20 ℃; for 48h; Inert atmosphere;

With sodium hydroxide; In tetrahydrofuran; water; at 20 ℃; for 2h;

DOI:10.1039/c0cc05840h

Reference yield: 92.0%

(1R,2R)-2-(bis(2-methoxybenzyl)carbamothioylthio)cyclohexylcarbamate (1292810-21-9) → (1R,2R)-2-aminocyclohexane-1-sulfonic acid (1076192-94-3)

Guidance literature:

With formic acid; dihydrogen peroxide; In water; at 20 ℃; for 72h; Inert atmosphere;

DOI:10.1039/c0cc05840h

upstream raw materials:

di-tert-butyl dicarbonate

(1R,2R)-2-(3,5-dinitrobenzamido)cyclohexyl bis(2-methoxybenzyl)carbamodithioate

Downstream raw materials:

(1R,2R)-2-aminocyclohexane-1-sulfonic acid