[3,4-bis-(4-methoxy-benzyloxy)-phenyl]-acetic acid 4-methoxy-benzyl ester

Base Information

Chemical Name:[3,4-bis-(4-methoxy-benzyloxy)-phenyl]-acetic acid 4-methoxy-benzyl ester
CAS No.:79248-60-5
Molecular Formula:C₃₂H₃₂O₇
Molecular Weight:528.602
Hs Code.:

Synonyms:[3,4-bis-(4-methoxy-benzyloxy)-phenyl]-acetic acid 4-methoxy-benzyl ester

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Chemical Property of [3,4-bis-(4-methoxy-benzyloxy)-phenyl]-acetic acid 4-methoxy-benzyl ester

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Technology Process of [3,4-bis-(4-methoxy-benzyloxy)-phenyl]-acetic acid 4-methoxy-benzyl ester

There total 1 articles about [3,4-bis-(4-methoxy-benzyloxy)-phenyl]-acetic acid 4-methoxy-benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 102-32-9
3,4-dihydroxyphenylacetate

: 824-94-2
p-methoxybenzyl chloride

: 79248-60-5
[3,4-bis-(4-methoxy-benzyloxy)-phenyl]-acetic acid 4-methoxy-benzyl ester

Guidance literature:: With tetrabutylammomium bromide; potassium carbonate; In acetone; for 96h; Heating;
DOI:10.1016/S0960-894X(99)00325-X

Reference yield: 90.0%

: 79248-60-5
[3,4-bis-(4-methoxy-benzyloxy)-phenyl]-acetic acid 4-methoxy-benzyl ester

: 229617-34-9
2-{3,4-bis[(4-methoxybenzyl)oxy]phenyl} acetic acid

Guidance literature:: With sodium hydroxide; In 1,4-dioxane;
DOI:10.1016/S0960-894X(99)00325-X

Reference yield:

: 79248-60-5
[3,4-bis-(4-methoxy-benzyloxy)-phenyl]-acetic acid 4-methoxy-benzyl ester

: (2S,3R,5R)-3-{2-[3,4-Bis-(4-methoxy-benzyloxy)-phenyl]-acetoxymethyl}-6-[1-carboxy-meth-(Z)-ylidene]-3-methyl-4,4,7-trioxo-4λ⁶-thia-1-aza-bicyclo[3.2.0]heptane-2-carboxylic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / aq.NaOH / dioxane

2: AgOAc / CH₂Cl₂

3: MCPBA

4: TFA / various solvent(s)

With sodium hydroxide; silver(I) acetate; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid; In 1,4-dioxane; dichloromethane;
DOI:10.1016/S0960-894X(99)00325-X