decamethylferrocenium tetrakis(3,5-bis(trifluoromethyl)phenyl)borate

Base Information

Chemical Name:decamethylferrocenium tetrakis(3,5-bis(trifluoromethyl)phenyl)borate
CAS No.:220517-48-6
Molecular Formula:C₂₀H₃₀Fe*C₃₂H₁₂BF₂₄
Molecular Weight:1189.53
Hs Code.:

Synonyms:decamethylferrocenium tetrakis(3,5-bis(trifluoromethyl)phenyl)borate

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Chemical Property of decamethylferrocenium tetrakis(3,5-bis(trifluoromethyl)phenyl)borate

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Technology Process of decamethylferrocenium tetrakis(3,5-bis(trifluoromethyl)phenyl)borate

There total 1 articles about decamethylferrocenium tetrakis(3,5-bis(trifluoromethyl)phenyl)borate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 12126-50-0
bis(pentamethylcyclopentadienyl)iron(II)

: 79060-88-1
sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate

: 220517-48-6
decamethylferrocenium tetrakis(3,5-bis(trifluoromethyl)phenyl)borate

Guidance literature:: bis(pentamethylcyclopentadienyl)iron(II); With silver tetrafluoroborate; In tetrahydrofuran; at -78 - 20 ℃; Schlenk technique; Inert atmosphere; Glovebox;

sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate; In tetrahydrofuran; dichloromethane; Schlenk technique; Inert atmosphere;
DOI:10.1002/chem.201900799

Reference yield: 73.0%

: 220517-48-6
decamethylferrocenium tetrakis(3,5-bis(trifluoromethyl)phenyl)borate

: [(1,2-bis(dimethylphosphino)ethane)4Cr2(C2Si(i-Pr)3)2(μ-N2)]

: 12126-50-0
bis(pentamethylcyclopentadienyl)iron(II)

: [(1,2-bis(dimethylphosphino)ethane)4Cr2(C2Si(i-Pr)3)2(μ-N2)][tetrakis(3,5-bis(trifluoromethylphenyl)borate]2

Guidance literature:: In diethyl ether; (N2); Schlenk technique; soln. of Fe complex in Et2O was added to stirred soln. of Cr complex in Et2O; stirred for 5 min; filtered through Celite; pentane added; filtered; washed (pentane); elem. anal.;
DOI:10.1021/ic101528d