1-(3,3-diphenylpropyl)-3-(3-hydroxymethylphenyl)-1-(2-morpholin-4-ylethyl)urea

Base Information

Chemical Name:1-(3,3-diphenylpropyl)-3-(3-hydroxymethylphenyl)-1-(2-morpholin-4-ylethyl)urea
CAS No.:938467-75-5
Molecular Formula:C₂₉H₃₅N₃O₃
Molecular Weight:473.615
Hs Code.:

Synonyms:1-(3,3-diphenylpropyl)-3-(3-hydroxymethylphenyl)-1-(2-morpholin-4-ylethyl)urea

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Chemical Property of 1-(3,3-diphenylpropyl)-3-(3-hydroxymethylphenyl)-1-(2-morpholin-4-ylethyl)urea

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Technology Process of 1-(3,3-diphenylpropyl)-3-(3-hydroxymethylphenyl)-1-(2-morpholin-4-ylethyl)urea

There total 10 articles about 1-(3,3-diphenylpropyl)-3-(3-hydroxymethylphenyl)-1-(2-morpholin-4-ylethyl)urea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 938467-15-3
3-[3-(3,3-diphenylpropyl)-3-(2-morpholin-4-ylethyl)ureido]benzoic acid methyl ester

: 938467-75-5
1-(3,3-diphenylpropyl)-3-(3-hydroxymethylphenyl)-1-(2-morpholin-4-ylethyl)urea

Guidance literature:: 3-[3-(3,3-diphenylpropyl)-3-(2-morpholin-4-ylethyl)ureido]benzoic acid methyl ester; With diisobutylaluminium hydride; In tetrahydrofuran; dichloromethane; at -78 - -27 ℃;

With lithium aluminium tetrahydride; In tetrahydrofuran; dichloromethane; at -78 - 0 ℃; for 1.5h;

With water; sodium tartrate; potassium tartrate; In tetrahydrofuran; dichloromethane; at 0 - 20 ℃; for 1h;

Reference yield:

: 4279-81-6
3,3-diphenylpropanal

: 938467-75-5
1-(3,3-diphenylpropyl)-3-(3-hydroxymethylphenyl)-1-(2-morpholin-4-ylethyl)urea

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogen / palladium 10% on activated carbon / ethanol / 16 h / 20 °C / 760.05 Torr

2.1: dichloromethane / 2 h / 20 °C

3.1: diisobutylaluminium hydride / tetrahydrofuran; dichloromethane / -78 - -27 °C

3.2: 1.5 h / -78 - 0 °C

3.3: 1 h / 0 - 20 °C

With hydrogen; diisobutylaluminium hydride; palladium 10% on activated carbon; In tetrahydrofuran; ethanol; dichloromethane;

Reference yield:

: 20017-67-8
3,3-diphenylpropan-1-ol

: 938467-75-5
1-(3,3-diphenylpropyl)-3-(3-hydroxymethylphenyl)-1-(2-morpholin-4-ylethyl)urea

Guidance literature:: Multi-step reaction with 4 steps

1.1: Dess-Martin periodane / dichloromethane / 1.5 h / 0 °C

2.1: hydrogen / palladium 10% on activated carbon / ethanol / 16 h / 20 °C / 760.05 Torr

3.1: dichloromethane / 2 h / 20 °C

4.1: diisobutylaluminium hydride / tetrahydrofuran; dichloromethane / -78 - -27 °C

4.2: 1.5 h / -78 - 0 °C

4.3: 1 h / 0 - 20 °C

With hydrogen; diisobutylaluminium hydride; Dess-Martin periodane; palladium 10% on activated carbon; In tetrahydrofuran; ethanol; dichloromethane;