2-chloro-N-phenyl-5-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-benzenesulfonamide

Base Information

Chemical Name:2-chloro-N-phenyl-5-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-benzenesulfonamide
CAS No.:1106313-73-8
Molecular Formula:C₁₈H₂₁BClNO₄S
Molecular Weight:393.699
Hs Code.:

Synonyms:2-chloro-N-phenyl-5-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-benzenesulfonamide

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Chemical Property of 2-chloro-N-phenyl-5-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-benzenesulfonamide

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Technology Process of 2-chloro-N-phenyl-5-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-benzenesulfonamide

There total 2 articles about 2-chloro-N-phenyl-5-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1106313-68-1
5-bromo-2-chloro-benzenesulfonic acid anilide

: 73183-34-3
bis(pinacol)diborane

: 1106313-73-8
2-chloro-N-phenyl-5-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-benzenesulfonamide

Guidance literature:: With potassium acetate; In 1,2-dimethoxyethane; at 90 ℃;

Reference yield:

: 60811-17-8
5-bromo-2-chloroaniline

: 1106313-73-8
2-chloro-N-phenyl-5-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-benzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogenchloride; sodium nitrite / water / 1 h / 0 °C

1.2: 2.25 h / 0 - 20 °C

2.1: pyridine / dichloromethane / 0.5 h

3.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate / 1,4-dioxane / 3 h / 90 °C / sealed tube

With pyridine; hydrogenchloride; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; sodium nitrite; In 1,4-dioxane; dichloromethane; water; 3.1: Suzuki-Miyaura cross-coupling;
DOI:10.1021/jm300403a

Reference yield:

: 1106313-73-8
2-chloro-N-phenyl-5-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-benzenesulfonamide

: 146940-37-6
3-amino-6-bromo-N-methylpyrazine-2-carboxamide

: 1377550-42-9
3-amino-6-(4-chloro-3-(N-phenylsulfamoyl)phenyl)-N-methylpyrazine-2-carboxamide

Guidance literature:: With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; triethylamine; In water; N,N-dimethyl-formamide; at 20 - 85 ℃; for 2h;
DOI:10.1021/jm300403a