L-alanyl-D-glutamic acid dibenzyl ester trifluoroacetate

Base Information

Chemical Name:L-alanyl-D-glutamic acid dibenzyl ester trifluoroacetate
CAS No.:66025-58-9
Molecular Formula:C₂HF₃O₂*C₂₂H₂₆N₂O₅
Molecular Weight:512.483
Hs Code.:

Synonyms:L-alanyl-D-glutamic acid dibenzyl ester trifluoroacetate

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Chemical Property of L-alanyl-D-glutamic acid dibenzyl ester trifluoroacetate

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Technology Process of L-alanyl-D-glutamic acid dibenzyl ester trifluoroacetate

There total 5 articles about L-alanyl-D-glutamic acid dibenzyl ester trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 59524-70-8,59524-71-9,85546-28-7
dibenzyl N-[N-(tert-butoxycarbonyl)-L-alanyl]-D-glutamate

: 76-05-1
trifluoroacetic acid

: 66025-58-9
L-alanyl-D-glutamic acid dibenzyl ester trifluoroacetate

Guidance literature:: In dichloromethane; at 20 ℃; for 40h; Inert atmosphere;
DOI:10.1021/ml2002746

Reference yield:

: 6893-26-1,21675-62-7,23009-64-5,25104-13-6,84960-48-5,25513-46-6
D-Glutamic acid

: 66025-58-9
L-alanyl-D-glutamic acid dibenzyl ester trifluoroacetate

Guidance literature:: Multi-step reaction with 3 steps

1.1: benzene / 26 h / Reflux

2.1: N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine / dichloromethane / 0.17 h / 20 °C / Inert atmosphere

2.2: 40 h / 20 °C / Inert atmosphere

3.1: dichloromethane / 40 h / 20 °C / Inert atmosphere

With N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; In dichloromethane; benzene;
DOI:10.1021/ml2002746

Reference yield:

: 104-15-4
toluene-4-sulfonic acid

: 66025-58-9
L-alanyl-D-glutamic acid dibenzyl ester trifluoroacetate

Guidance literature:: Multi-step reaction with 3 steps

1.1: benzene / 26 h / Reflux

2.1: N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine / dichloromethane / 0.17 h / 20 °C / Inert atmosphere

2.2: 40 h / 20 °C / Inert atmosphere

3.1: dichloromethane / 40 h / 20 °C / Inert atmosphere

With N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; In dichloromethane; benzene;
DOI:10.1021/ml2002746