N⁴-[3-(1-{[tert-butyldimethylsilyl]oxy}cyclohexyl)propyl]quinolin-3,4-diamine

Base Information

• Chemical Name: N⁴-[3-(1-{[tert-butyldimethylsilyl]oxy}cyclohexyl)propyl]quinolin-3,4-diamine
• CAS No.: 879514-64-4
• Molecular Formula: C₂₄H₃₉N₃OSi
• Molecular Weight: 413.679

Synonyms:N⁴-[3-(1-{[tert-butyldimethylsilyl]oxy}cyclohexyl)propyl]quinolin-3,4-diamine

Chemical Property of N⁴-[3-(1-{[tert-butyldimethylsilyl]oxy}cyclohexyl)propyl]quinolin-3,4-diamine

Chemical Property:

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Technology Process of N⁴-[3-(1-{[tert-butyldimethylsilyl]oxy}cyclohexyl)propyl]quinolin-3,4-diamine

There total 1 articles about N⁴-[3-(1-{[tert-butyldimethylsilyl]oxy}cyclohexyl)propyl]quinolin-3,4-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-[3-(1-{[tert-butyldimethylsilyl]oxy}cyclohexyl)propyl]-3-nitroquinolin-4-amine (879514-33-7) → N4-[3-(1-{[tert-butyldimethylsilyl]oxy}cyclohexyl)propyl]quinolin-3,4-diamine (879514-64-4)

Guidance literature:

With hydrogen; 5 % platinum on carbon; In ethyl acetate; for 2h; under 1551.49 Torr;

Reference yield:

N4-[3-(1-{[tert-butyldimethylsilyl]oxy}cyclohexyl)propyl]quinolin-3,4-diamine (879514-64-4) + ethoxyacetyl chloride (14077-58-8) → N-(4-{[3-(1-{[tert-butyldimethylsilyl]oxy}cyclohexyl)propyl]amino}quinolin-3-yl)-2-ethoxyacetamide hydrochloride

Guidance literature:

In dichloromethane; at 0 ℃; for 1h;

Reference yield:

N4-[3-(1-{[tert-butyldimethylsilyl]oxy}cyclohexyl)propyl]quinolin-3,4-diamine (879514-64-4) + 1,1,1-trimethoxybutane (43083-12-1) → 1-{3-[1-(tert-butyldimethylsilanyloxy)cyclohexyl]propyl}-2-propyl-1H-imidazo[4,5-c]quinoline

Guidance literature:

With pyridine hydrochloride; In toluene; for 2h; Heating / reflux;

upstream raw materials:

N-[3-(1-{[tert-butyldimethylsilyl]oxy}cyclohexyl)propyl]-3-nitroquinolin-4-amine

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