10,19-Dibenzyl-1,4,13,16-tetraoxa-7,10,19,22-tetraazacyclotetracosane-6,23-dione

Base Information

Chemical Name:10,19-Dibenzyl-1,4,13,16-tetraoxa-7,10,19,22-tetraazacyclotetracosane-6,23-dione
CAS No.:147714-35-0
Molecular Formula:C₃₀H₄₄N₄O₆
Molecular Weight:556.703
Hs Code.:

Synonyms:10,19-Dibenzyl-1,4,13,16-tetraoxa-7,10,19,22-tetraazacyclotetracosane-6,23-dione

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Chemical Property of 10,19-Dibenzyl-1,4,13,16-tetraoxa-7,10,19,22-tetraazacyclotetracosane-6,23-dione

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Technology Process of 10,19-Dibenzyl-1,4,13,16-tetraoxa-7,10,19,22-tetraazacyclotetracosane-6,23-dione

There total 3 articles about 10,19-Dibenzyl-1,4,13,16-tetraoxa-7,10,19,22-tetraazacyclotetracosane-6,23-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 28.0%

: 31255-09-1
3,6-dioxa-1,8-octanoyl dichloride

: 147688-23-1
1,14-Diamino-3,12-dibenzyl-6,9-dioxa-3,12-diazatetradecane

: 147714-35-0
10,19-Dibenzyl-1,4,13,16-tetraoxa-7,10,19,22-tetraazacyclotetracosane-6,23-dione

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; toluene; at 60 ℃; for 144h;

Reference yield:

: 66582-26-1
1,10-dibenzyl-4,7-dioxa-1,10-diazadecane

: 147714-35-0
10,19-Dibenzyl-1,4,13,16-tetraoxa-7,10,19,22-tetraazacyclotetracosane-6,23-dione

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / acetonitrile; toluene / 72 h / 80 °C

2: 98 percent / H₂ / 10percent Pd/C / methanol

3: 28 percent / Et₃N / toluene; dimethylformamide / 144 h / 60 °C

With hydrogen; triethylamine; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide; toluene; acetonitrile;

Reference yield:

: 147688-22-0
3,12-Dibenzyl-1,14-bis(benzyloxycarbonylamino)-6,9-dioxa-3,12-diazatetradecane

: 147714-35-0
10,19-Dibenzyl-1,4,13,16-tetraoxa-7,10,19,22-tetraazacyclotetracosane-6,23-dione

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / H₂ / 10percent Pd/C / methanol

2: 28 percent / Et₃N / toluene; dimethylformamide / 144 h / 60 °C

With hydrogen; triethylamine; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide; toluene;