3,12-Dibenzyl-1,14-bis(benzyloxycarbonylamino)-6,9-dioxa-3,12-diazatetradecane

Base Information

Chemical Name:3,12-Dibenzyl-1,14-bis(benzyloxycarbonylamino)-6,9-dioxa-3,12-diazatetradecane
CAS No.:147688-22-0
Molecular Formula:C₄₀H₅₀N₄O₆
Molecular Weight:682.86
Hs Code.:

Synonyms:3,12-Dibenzyl-1,14-bis(benzyloxycarbonylamino)-6,9-dioxa-3,12-diazatetradecane

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Chemical Property of 3,12-Dibenzyl-1,14-bis(benzyloxycarbonylamino)-6,9-dioxa-3,12-diazatetradecane

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Technology Process of 3,12-Dibenzyl-1,14-bis(benzyloxycarbonylamino)-6,9-dioxa-3,12-diazatetradecane

There total 1 articles about 3,12-Dibenzyl-1,14-bis(benzyloxycarbonylamino)-6,9-dioxa-3,12-diazatetradecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 25711-25-5
benzyl aziridine-1-carboxylate

: 66582-26-1
1,10-dibenzyl-4,7-dioxa-1,10-diazadecane

: 147688-22-0
3,12-Dibenzyl-1,14-bis(benzyloxycarbonylamino)-6,9-dioxa-3,12-diazatetradecane

Guidance literature:: In toluene; acetonitrile; at 80 ℃; for 72h;

Reference yield: 98.0%

: 147688-22-0
3,12-Dibenzyl-1,14-bis(benzyloxycarbonylamino)-6,9-dioxa-3,12-diazatetradecane

: 147688-23-1
1,14-Diamino-3,12-dibenzyl-6,9-dioxa-3,12-diazatetradecane

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol;

Reference yield:

: 147688-22-0
3,12-Dibenzyl-1,14-bis(benzyloxycarbonylamino)-6,9-dioxa-3,12-diazatetradecane

: 147688-24-2
10,19-Dibenzyl-1,4,13,16-tetraoxa-7,10,19,22-tetraazacyclotetracosane

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / H₂ / 10percent Pd/C / methanol

2: 28 percent / Et₃N / toluene; dimethylformamide / 144 h / 60 °C

3: 91 percent / LiAlH₄ / tetrahydrofuran / 18 h / Heating

With lithium aluminium tetrahydride; hydrogen; triethylamine; palladium on activated charcoal; In tetrahydrofuran; methanol; N,N-dimethyl-formamide; toluene;