10-benzoylanhydroartemisinin

Base Information

Chemical Name:10-benzoylanhydroartemisinin
CAS No.:226952-29-0
Molecular Formula:C₂₂H₂₆O₅
Molecular Weight:370.445
Hs Code.:

Synonyms:10-benzoylanhydroartemisinin

Suppliers and Price of 10-benzoylanhydroartemisinin

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 10-benzoylanhydroartemisinin

Chemical Property:

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Technology Process of 10-benzoylanhydroartemisinin

There total 4 articles about 10-benzoylanhydroartemisinin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 226952-30-3
C₂₂H₂₈O₅

: 226952-29-0
10-benzoylanhydroartemisinin

Guidance literature:: With N-methyl-2-indolinone; tetrapropylammonium perruthennate; 4 Angstroems MS; In dichloromethane; for 2h; Ambient temperature;
DOI:10.1016/S0040-4020(98)01170-3

Reference yield:

: 100-58-3
phenylmagnesium bromide

: 226952-29-0
10-benzoylanhydroartemisinin

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / tetrahydrofuran / 2 h / -78 °C

2: 97 percent / TPAP, 4 Angstroems MS, NMO / CH₂Cl₂ / 2 h / Ambient temperature

With N-methyl-2-indolinone; tetrapropylammonium perruthennate; 4 Angstroems MS; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0040-4020(98)01170-3

Reference yield:

: 226952-18-7
10-formylanhydroartemisinin

: 226952-29-0
10-benzoylanhydroartemisinin

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / tetrahydrofuran / 2 h / -78 °C

2: 97 percent / TPAP, 4 Angstroems MS, NMO / CH₂Cl₂ / 2 h / Ambient temperature

With N-methyl-2-indolinone; tetrapropylammonium perruthennate; 4 Angstroems MS; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0040-4020(98)01170-3