C₄₇H₆₀N₂O₉

Base Information

Chemical Name:C₄₇H₆₀N₂O₉
CAS No.:1270942-87-4
Molecular Formula:C₄₇H₆₀N₂O₉
Molecular Weight:797.001
Hs Code.:

C<sub>47</sub>H<sub>60</sub>N<sub>2</sub>O<sub>9</sub>

Synonyms:C₄₇H₆₀N₂O₉

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Chemical Property of C₄₇H₆₀N₂O₉

Chemical Property:

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Technology Process of C₄₇H₆₀N₂O₉

There total 17 articles about C₄₇H₆₀N₂O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 1270942-86-3
(3E,6S,7S,8R,9Z)-12-{2,5-dimethoxy-3-[(3R,4E)-3-methoxyhepta-4,6-dienamido]phe-nyl}-8-(4-methoxybenzyloxy)-7,9-dimethyldodeca-1,3,9-trien-6-yl1-[(cyclohex-1-ene)amido]cyclopropane-1-carboxylate

: 1270942-87-4
C₄₇H₆₀N₂O₉

Guidance literature:: With dichloro(3-phenyl-1H-inden-1-ylidene)bis(tricyclohexylphosphine)ruthenium(II); In dichloromethane; at 25 - 40 ℃; Inert atmosphere; Darkness;
DOI:10.1021/ol200160p

Reference yield:

: 1270942-93-2
2,5-dimethoxy-1-nitro-3-vinylbenzene

: 1270942-87-4
C₄₇H₆₀N₂O₉

Guidance literature:: Multi-step reaction with 10 steps

1.1: bis(1,5-cyclooctadiene)diiridium(I) dichloride; 1,2-bis-(diphenylphosphino)ethane / 1,2-dichloro-ethane; toluene / 14 h / 25 °C / Inert atmosphere

2.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; sodium hydroxide / tetrahydrofuran; water / 25 h / 50 °C / Inert atmosphere; Sealed tube

3.1: periodic acid / ethyl acetate / 0.67 h / 25 °C

4.1: dimethylaluminum chloride / hexane; dichloromethane / 0.17 h / -78 °C / Inert atmosphere

4.2: 5 h / -78 °C / Inert atmosphere

5.1: dmap; triethylamine / dichloromethane; toluene / 1 h / 0 °C

6.1: 1.3-propanedithiol; triethylamine / methanol / 22 h / 25 °C

7.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 24 h / 25 °C / Inert atmosphere

8.1: sulfur; sodium tetrahydroborate / tetrahydrofuran / 1 h / 50 °C / Inert atmosphere

9.1: bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; N-ethyl-N,N-diisopropylamine / tetrahydrofuran; toluene / 21 h / 25 °C / Molecular sieve; Inert atmosphere

10.1: dichloro(3-phenyl-1H-inden-1-ylidene)bis(tricyclohexylphosphine)ruthenium(II) / dichloromethane / 25 - 40 °C / Inert atmosphere; Darkness

With 1.3-propanedithiol; sulfur; dmap; sodium tetrahydroborate; bis(1,5-cyclooctadiene)diiridium(I) dichloride; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; dichloro(3-phenyl-1H-inden-1-ylidene)bis(tricyclohexylphosphine)ruthenium(II); bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; dimethylaluminum chloride; periodic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; 1,2-bis-(diphenylphosphino)ethane; sodium hydroxide; In tetrahydrofuran; methanol; hexane; dichloromethane; water; ethyl acetate; 1,2-dichloro-ethane; toluene; 1.1: Suzuki-Miyaura coupling / 2.1: Suzuki coupling;
DOI:10.1021/ol200160p

Reference yield:

: 1270942-89-6
2-(2,5-dimethoxy-3-nitrophenethyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 1270942-87-4
C₄₇H₆₀N₂O₉

Guidance literature:: Multi-step reaction with 9 steps

1.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; sodium hydroxide / tetrahydrofuran; water / 25 h / 50 °C / Inert atmosphere; Sealed tube

2.1: periodic acid / ethyl acetate / 0.67 h / 25 °C

3.1: dimethylaluminum chloride / hexane; dichloromethane / 0.17 h / -78 °C / Inert atmosphere

3.2: 5 h / -78 °C / Inert atmosphere

4.1: dmap; triethylamine / dichloromethane; toluene / 1 h / 0 °C

5.1: 1.3-propanedithiol; triethylamine / methanol / 22 h / 25 °C

6.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 24 h / 25 °C / Inert atmosphere

7.1: sulfur; sodium tetrahydroborate / tetrahydrofuran / 1 h / 50 °C / Inert atmosphere

8.1: bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; N-ethyl-N,N-diisopropylamine / tetrahydrofuran; toluene / 21 h / 25 °C / Molecular sieve; Inert atmosphere

9.1: dichloro(3-phenyl-1H-inden-1-ylidene)bis(tricyclohexylphosphine)ruthenium(II) / dichloromethane / 25 - 40 °C / Inert atmosphere; Darkness

With 1.3-propanedithiol; sulfur; dmap; sodium tetrahydroborate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; dichloro(3-phenyl-1H-inden-1-ylidene)bis(tricyclohexylphosphine)ruthenium(II); bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; dimethylaluminum chloride; periodic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In tetrahydrofuran; methanol; hexane; dichloromethane; water; ethyl acetate; toluene; 1.1: Suzuki coupling;
DOI:10.1021/ol200160p