2,3-di-O-benzyl-1,5-dideoxy-1,5-imino-4-O-(1-naphthyl)methyl-6-O-sulfo-N-(4-nitro)benzenesulfonyl-L-iditol sodium salt

Base Information

Chemical Name:2,3-di-O-benzyl-1,5-dideoxy-1,5-imino-4-O-(1-naphthyl)methyl-6-O-sulfo-N-(4-nitro)benzenesulfonyl-L-iditol sodium salt
CAS No.:1207750-75-1
Molecular Formula:C₃₇H₃₅N₂O₁₁S₂*Na
Molecular Weight:770.813
Hs Code.:

Synonyms:2,3-di-O-benzyl-1,5-dideoxy-1,5-imino-4-O-(1-naphthyl)methyl-6-O-sulfo-N-(4-nitro)benzenesulfonyl-L-iditol sodium salt

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Chemical Property of 2,3-di-O-benzyl-1,5-dideoxy-1,5-imino-4-O-(1-naphthyl)methyl-6-O-sulfo-N-(4-nitro)benzenesulfonyl-L-iditol sodium salt

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Technology Process of 2,3-di-O-benzyl-1,5-dideoxy-1,5-imino-4-O-(1-naphthyl)methyl-6-O-sulfo-N-(4-nitro)benzenesulfonyl-L-iditol sodium salt

There total 1 articles about 2,3-di-O-benzyl-1,5-dideoxy-1,5-imino-4-O-(1-naphthyl)methyl-6-O-sulfo-N-(4-nitro)benzenesulfonyl-L-iditol sodium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1207750-73-9
2,3-di-O-benzyl-1,5-dideoxy-1,5-imino-4-O-(1-naphthyl)methyl-N-(4-nitro)benzenesulfonyl-L-iditol

: 1207750-75-1
2,3-di-O-benzyl-1,5-dideoxy-1,5-imino-4-O-(1-naphthyl)methyl-6-O-sulfo-N-(4-nitro)benzenesulfonyl-L-iditol sodium salt

Guidance literature:: 2,3-di-O-benzyl-1,5-dideoxy-1,5-imino-4-O-(1-naphthyl)methyl-N-(4-nitro)benzenesulfonyl-L-iditol; With sulfur trioxide pyridine complex; In N,N-dimethyl-formamide; at 20 ℃; for 0.25h;

With sodium hydrogencarbonate; In water; N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2009.11.042

Reference yield: 93.0%

: 1207750-75-1
2,3-di-O-benzyl-1,5-dideoxy-1,5-imino-4-O-(1-naphthyl)methyl-6-O-sulfo-N-(4-nitro)benzenesulfonyl-L-iditol sodium salt

: 1207750-76-2
2,3-di-O-benzyl-4-O-(1-naphthyl)methyl-6-O-sulfo-1,5-dideoxy-1,5-imino-L-iditol sodium salt

Guidance literature:: With thiophenol; triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 144h; pH=9 - 10;
DOI:10.1016/j.tetlet.2009.11.042