(S)-methyl 3-(dibenzylamino)-2-morpholinopropanoate

Base Information

Chemical Name:(S)-methyl 3-(dibenzylamino)-2-morpholinopropanoate
CAS No.:888957-43-5
Molecular Formula:C₂₂H₂₈N₂O₃
Molecular Weight:368.476
Hs Code.:

Synonyms:(S)-methyl 3-(dibenzylamino)-2-morpholinopropanoate

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Chemical Property of (S)-methyl 3-(dibenzylamino)-2-morpholinopropanoate

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Technology Process of (S)-methyl 3-(dibenzylamino)-2-morpholinopropanoate

There total 4 articles about (S)-methyl 3-(dibenzylamino)-2-morpholinopropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 110-91-8,99108-56-2
morpholine

: 888957-31-1
(R)-2-(methoxycarbonyl)-2-(dibenzylamino)ethyl methanesulfonate

: 888957-43-5
(S)-methyl 3-(dibenzylamino)-2-morpholinopropanoate

Guidance literature:: In acetonitrile; at 60 ℃;
DOI:10.1021/ol060700u

Reference yield: 77.0%

: 110-91-8,99108-56-2
morpholine

: 202478-34-0
(R)-methyl 2-(dibenzylamino)-3-hydroxypropanoate

: 888957-43-5
(S)-methyl 3-(dibenzylamino)-2-morpholinopropanoate

Guidance literature:: (R)-methyl 2-(dibenzylamino)-3-hydroxypropanoate; With triethylamine; Methanesulfonic anhydride; In acetonitrile; at 20 ℃;

morpholine; In acetonitrile; at 60 ℃;
DOI:10.1021/ol060700u

Reference yield:

: 100-39-0
benzyl bromide

: 888957-43-5
(S)-methyl 3-(dibenzylamino)-2-morpholinopropanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: 95 percent / sodium hydrogen carbonate / tetrahydrofuran; dimethylsulfoxide / 15 h / Heating

2.1: Ms₂O; triethylamine / acetonitrile / 20 °C

2.2: 77 percent / acetonitrile / 60 °C

With sodium hydrogencarbonate; triethylamine; Methanesulfonic anhydride; In tetrahydrofuran; dimethyl sulfoxide; acetonitrile;
DOI:10.1021/ol060700u