Bis(2-methoxyethyl) phthalate

Base Information

• Chemical Name: Bis(2-methoxyethyl) phthalate
• CAS No.: 117-82-8
• Molecular Formula: C14H18O6
• Molecular Weight: 282.293
• Hs Code.: 29173490
• European Community (EC) Number: 204-212-6
• NSC Number: 2147
• UNII: 68W8XUO221
• DSSTox Substance ID: DTXSID8025094
• Nikkaji Number: J3.615C
• Wikipedia: Bis(2-methoxyethyl) phthalate
• Wikidata: Q15632774
• Metabolomics Workbench ID: 123281
• ChEMBL ID: CHEMBL1302251
• Mol file: 117-82-8.mol

Synonyms:di(2-methoxyethyl)phthalate;dimethoxyethyl phthalate

Chemical Property of Bis(2-methoxyethyl) phthalate

Chemical Property:

• Appearance/Colour: Practically colorless, oily liq. Very slight.
• Vapor Pressure: 1.01E-07mmHg at 25°C
• Melting Point: -42.4°C
• Refractive Index: n20/D 1.503
• Boiling Point: 312.457 °C at 760 mmHg
• Flash Point: 131.61 °C
• PSA: 71.06000
• Density: 1.157 g/cm³
• LogP: 1.29300
• Storage Temp.: Refrigerator
• Solubility.: Chloroform (Slightly), Ethyl Acetate (Slightly)
• Water Solubility.: Soluble in water 8500 mg/L at 25°C.
• XLogP3: 1.4
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 6
• Rotatable Bond Count: 10
• Exact Mass: 282.11033829
• Heavy Atom Count: 20
• Complexity: 274

Purity/Quality:

99% ^*data from raw suppliers

Bis(2-methoxyethyl) Phthalate ^*data from reagent suppliers

Safty Information:

• Pictogram(s): T
• Hazard Codes: T
• Statements: 61-62
• Safety Statements: 53-45

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Chemical Classes: Plastics & Rubber -> Phthalate Esters
• Canonical SMILES: COCCOC(=O)C1=CC=CC=C1C(=O)OCCOC
• Uses: Bis(2-methoxyethyl) Phthalate is a phthalate derivative found in cosmetic products. Plasticizer; solvent It finds it application in cosmetic industry. It is also used as a plasticizer for toys, including inflatable water products, hoppers, play and exercise balls.

Technology Process of Bis(2-methoxyethyl) phthalate

There total 2 articles about Bis(2-methoxyethyl) phthalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

phthalic anhydride (85-44-9) + 2-methoxy-ethanol (109-86-4,95507-80-5) → bis(2-methoxyethyl) phthalate (117-82-8)

Guidance literature:

With diacidic ionic liquid supported on magnetic-silica nanoparticles; In neat (no solvent); at 130 ℃; for 8h; Dean-Stark;

DOI:10.1007/s13738-018-1450-8

Reference yield:

2-methoxy-ethanol (109-86-4,95507-80-5) + Phthaloyl dichloride (88-95-9) → bis(2-methoxyethyl) phthalate (117-82-8)

Guidance literature:

With triethylamine; In diethyl ether; at 0 ℃;

DOI:10.1021/jo020753z

Reference yield:

bis(2-methoxyethyl) phthalate (117-82-8) → C12H12O4(2+)

Guidance literature:

With trifluorormethanesulfonic acid; at 60 ℃;

DOI:10.1021/jo020753z

upstream raw materials:

phthalic anhydride

2-methoxy-ethanol

Phthaloyl dichloride

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