chlorhydrate d'aspartyl (β-para-nitrobenzyle ester) aspartate (β-para-nitrobenzyle ester) de methyl

Base Information

Chemical Name:chlorhydrate d'aspartyl (β-para-nitrobenzyle ester) aspartate (β-para-nitrobenzyle ester) de methyl
CAS No.:66215-99-4
Molecular Formula:C₂₃H₂₄N₄O₁₁*ClH
Molecular Weight:568.925
Hs Code.:

Synonyms:chlorhydrate d'aspartyl (β-para-nitrobenzyle ester) aspartate (β-para-nitrobenzyle ester) de methyl

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Chemical Property of chlorhydrate d'aspartyl (β-para-nitrobenzyle ester) aspartate (β-para-nitrobenzyle ester) de methyl

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Technology Process of chlorhydrate d'aspartyl (β-para-nitrobenzyle ester) aspartate (β-para-nitrobenzyle ester) de methyl

There total 3 articles about chlorhydrate d'aspartyl (β-para-nitrobenzyle ester) aspartate (β-para-nitrobenzyle ester) de methyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 30925-21-4
N-tertiobutyloxycarbonyl-β-aspartate de para-nitrobenzyle

: 66215-99-4
chlorhydrate d'aspartyl (β-para-nitrobenzyle ester) aspartate (β-para-nitrobenzyle ester) de methyl

Guidance literature:: Multi-step reaction with 4 steps

1: 95.5 percent / ethyl acetate / 0.08 h

2: 91 percent / HCl(g) / ethyl acetate / 2.5 h

3: 66.5 percent / dicyclohexylcarbodiimide / CHCl₃ / 2 h, -10 deg C then 3 h, room temperature

4: HCl(g) / CHCl₃ / 2 h

With hydrogenchloride; dicyclohexyl-carbodiimide; In chloroform; ethyl acetate;

Reference yield:

: 66215-90-5
N-tertiobutyloxycarbonyl aspartate (β-para-nitrobenzyle ester) de methyl

: 66215-99-4
chlorhydrate d'aspartyl (β-para-nitrobenzyle ester) aspartate (β-para-nitrobenzyle ester) de methyl

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / HCl(g) / ethyl acetate / 2.5 h

2: 66.5 percent / dicyclohexylcarbodiimide / CHCl₃ / 2 h, -10 deg C then 3 h, room temperature

3: HCl(g) / CHCl₃ / 2 h

With hydrogenchloride; dicyclohexyl-carbodiimide; In chloroform; ethyl acetate;

Reference yield:

: 66215-93-8
chlorhydrate d'aspartate (β-para-nitrobenzyle ester) de methyl

: 66215-99-4
chlorhydrate d'aspartyl (β-para-nitrobenzyle ester) aspartate (β-para-nitrobenzyle ester) de methyl

Guidance literature:: Multi-step reaction with 2 steps

1: 66.5 percent / dicyclohexylcarbodiimide / CHCl₃ / 2 h, -10 deg C then 3 h, room temperature

2: HCl(g) / CHCl₃ / 2 h

With hydrogenchloride; dicyclohexyl-carbodiimide; In chloroform;