N-acetyle aspartyl (β-para-nitrobenzyle ester) aspartate (β-para-nitrobenzyle ester) de methyl

Base Information

Chemical Name:N-acetyle aspartyl (β-para-nitrobenzyle ester) aspartate (β-para-nitrobenzyle ester) de methyl
CAS No.:66215-85-8
Molecular Formula:C₂₅H₂₆N₄O₁₂
Molecular Weight:574.501
Hs Code.:

Synonyms:N-acetyle aspartyl (β-para-nitrobenzyle ester) aspartate (β-para-nitrobenzyle ester) de methyl

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Chemical Property of N-acetyle aspartyl (β-para-nitrobenzyle ester) aspartate (β-para-nitrobenzyle ester) de methyl

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Technology Process of N-acetyle aspartyl (β-para-nitrobenzyle ester) aspartate (β-para-nitrobenzyle ester) de methyl

There total 5 articles about N-acetyle aspartyl (β-para-nitrobenzyle ester) aspartate (β-para-nitrobenzyle ester) de methyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 66215-99-4
chlorhydrate d'aspartyl (β-para-nitrobenzyle ester) aspartate (β-para-nitrobenzyle ester) de methyl

: 75-36-5
acetyl chloride

: 66215-85-8
N-acetyle aspartyl (β-para-nitrobenzyle ester) aspartate (β-para-nitrobenzyle ester) de methyl

Guidance literature:: With triethylamine; In chloroform; 10 min, 0 deg C then 1 h, room temperature;

Reference yield:

: 30925-21-4
N-tertiobutyloxycarbonyl-β-aspartate de para-nitrobenzyle

: 66215-85-8
N-acetyle aspartyl (β-para-nitrobenzyle ester) aspartate (β-para-nitrobenzyle ester) de methyl

Guidance literature:: Multi-step reaction with 5 steps

1: 95.5 percent / ethyl acetate / 0.08 h

2: 91 percent / HCl(g) / ethyl acetate / 2.5 h

3: 66.5 percent / dicyclohexylcarbodiimide / CHCl₃ / 2 h, -10 deg C then 3 h, room temperature

4: HCl(g) / CHCl₃ / 2 h

5: 85 percent / triethylamine / CHCl₃ / 10 min, 0 deg C then 1 h, room temperature

With hydrogenchloride; triethylamine; dicyclohexyl-carbodiimide; In chloroform; ethyl acetate;

Reference yield:

: 66215-90-5
N-tertiobutyloxycarbonyl aspartate (β-para-nitrobenzyle ester) de methyl

: 66215-85-8
N-acetyle aspartyl (β-para-nitrobenzyle ester) aspartate (β-para-nitrobenzyle ester) de methyl

Guidance literature:: Multi-step reaction with 4 steps

1: 91 percent / HCl(g) / ethyl acetate / 2.5 h

2: 66.5 percent / dicyclohexylcarbodiimide / CHCl₃ / 2 h, -10 deg C then 3 h, room temperature

3: HCl(g) / CHCl₃ / 2 h

4: 85 percent / triethylamine / CHCl₃ / 10 min, 0 deg C then 1 h, room temperature

With hydrogenchloride; triethylamine; dicyclohexyl-carbodiimide; In chloroform; ethyl acetate;