(1S,2S,3R,4R)-1-hydroxy-2,3-(4-methoxybenzylidenedioxy)-4-{[(4-methoxyphenyl)diphenylmethoxy]methyl}-5-methylenecyclopentane

Base Information

Chemical Name:(1S,2S,3R,4R)-1-hydroxy-2,3-(4-methoxybenzylidenedioxy)-4-{[(4-methoxyphenyl)diphenylmethoxy]methyl}-5-methylenecyclopentane
CAS No.:851935-76-7
Molecular Formula:C₃₅H₃₄O₆
Molecular Weight:550.651
Hs Code.:

Synonyms:(1S,2S,3R,4R)-1-hydroxy-2,3-(4-methoxybenzylidenedioxy)-4-{[(4-methoxyphenyl)diphenylmethoxy]methyl}-5-methylenecyclopentane

Suppliers and Price of (1S,2S,3R,4R)-1-hydroxy-2,3-(4-methoxybenzylidenedioxy)-4-{[(4-methoxyphenyl)diphenylmethoxy]methyl}-5-methylenecyclopentane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1S,2S,3R,4R)-1-hydroxy-2,3-(4-methoxybenzylidenedioxy)-4-{[(4-methoxyphenyl)diphenylmethoxy]methyl}-5-methylenecyclopentane

Chemical Property:

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Technology Process of (1S,2S,3R,4R)-1-hydroxy-2,3-(4-methoxybenzylidenedioxy)-4-{[(4-methoxyphenyl)diphenylmethoxy]methyl}-5-methylenecyclopentane

There total 1 articles about (1S,2S,3R,4R)-1-hydroxy-2,3-(4-methoxybenzylidenedioxy)-4-{[(4-methoxyphenyl)diphenylmethoxy]methyl}-5-methylenecyclopentane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 851935-67-6
(1S,2R,3R,4R)-1-ethoxycarbonyloxy-2,3-(p-methoxybenzylidenedioxy)-4-{[(4-methoxyphenyl)diphenylmethoxy]methyl}-5-methylenecyclopentane

: 851935-76-7
(1S,2S,3R,4R)-1-hydroxy-2,3-(4-methoxybenzylidenedioxy)-4-{[(4-methoxyphenyl)diphenylmethoxy]methyl}-5-methylenecyclopentane

Guidance literature:: With sodium methylate; In tetrahydrofuran; methanol; at 20 ℃; for 5h;
DOI:10.1039/b418829b

Reference yield: 79.0%

: 851935-76-7
(1S,2S,3R,4R)-1-hydroxy-2,3-(4-methoxybenzylidenedioxy)-4-{[(4-methoxyphenyl)diphenylmethoxy]methyl}-5-methylenecyclopentane

: 87-42-3
6-chloropurine

: 851935-78-9
9-{(1R,2S,3R,4R)-2,3-(4-methoxybenzylidenedioxy)-4-{[(4-methoxyphenyl)diphenylmethoxy]methyl}-5-methylenencyclopentan-1-yl}-6-chloropurine

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 0 - 20 ℃; for 21h;
DOI:10.1039/b418829b

Reference yield:

: 851935-76-7
(1S,2S,3R,4R)-1-hydroxy-2,3-(4-methoxybenzylidenedioxy)-4-{[(4-methoxyphenyl)diphenylmethoxy]methyl}-5-methylenecyclopentane

: 603-35-0
triphenylphosphine

: 700-49-2
2-fluoroadenine

: 2-Fluoro-9-{(2R,3aS,4R,6R,6aR)-2-(4-methoxy-phenyl)-6-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-5-methylene-tetrahydro-cyclopenta[1,3]dioxol-4-yl}-9H-purin-6-ylamine

: C₅₈H₄₉FN₅O₅P

Guidance literature:: With di-isopropyl azodicarboxylate; In tetrahydrofuran; at 0 - 20 ℃; for 21h; Title compound not separated from byproducts;
DOI:10.1039/b418829b