methyl 4-[6-(2-thienyl)[1,2,4]triazolo[3,4-b][1,3,4]thiadiazol-3-yl]phenyl ether

Base Information

Chemical Name:methyl 4-[6-(2-thienyl)[1,2,4]triazolo[3,4-b][1,3,4]thiadiazol-3-yl]phenyl ether
CAS No.:577700-42-6
Molecular Formula:C₁₄H₁₀N₄OS₂
Molecular Weight:314.392
Hs Code.:
Mol file:577700-42-6.mol

Synonyms:3-(4-methoxyphenyl)-6-(thiophen-2-yl)-[1,2,4]triazolo[3,4-b][1,3,4]thiadiazole

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Chemical Property of methyl 4-[6-(2-thienyl)[1,2,4]triazolo[3,4-b][1,3,4]thiadiazol-3-yl]phenyl ether

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Technology Process of methyl 4-[6-(2-thienyl)[1,2,4]triazolo[3,4-b][1,3,4]thiadiazol-3-yl]phenyl ether

There total 5 articles about methyl 4-[6-(2-thienyl)[1,2,4]triazolo[3,4-b][1,3,4]thiadiazol-3-yl]phenyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 527-72-0
2-thiophenylcarboxylic acid

: 36209-49-1
4-amino-5-(4-methoxyphenyl)-2,3-dihydro-4H-1,2,4-triazole-3-thione

: 577700-42-6
3-(4-methoxyphenyl)-6-(thiophen-2-yl)-[1,2,4]triazolo[3,4-b][1,3,4]thiadiazole

Guidance literature:: With trichlorophosphate; Reflux;
DOI:10.5012/bkcs.2012.33.12.4180

Reference yield:

: 57486-67-6
methyl o-fluorophenylacetate

: 577700-42-6
3-(4-methoxyphenyl)-6-(thiophen-2-yl)-[1,2,4]triazolo[3,4-b][1,3,4]thiadiazole

Guidance literature:: Multi-step reaction with 4 steps

1: hydrazine hydrate / methanol / Reflux

2: potassium hydroxide / methanol / 0 - 5 °C / Reflux

3: hydrazine hydrate / water / Reflux

4: trichlorophosphate / Reflux

With hydrazine hydrate; potassium hydroxide; trichlorophosphate; In methanol; water;
DOI:10.5012/bkcs.2012.33.12.4180

Reference yield:

: 451-82-1
(2-fluorophenyl)acetic acid

: 577700-42-6
3-(4-methoxyphenyl)-6-(thiophen-2-yl)-[1,2,4]triazolo[3,4-b][1,3,4]thiadiazole

Guidance literature:: Multi-step reaction with 5 steps

1: sulfuric acid / Reflux

2: hydrazine hydrate / methanol / Reflux

3: potassium hydroxide / methanol / 0 - 5 °C / Reflux

4: hydrazine hydrate / water / Reflux

5: trichlorophosphate / Reflux

With sulfuric acid; hydrazine hydrate; potassium hydroxide; trichlorophosphate; In methanol; water;
DOI:10.5012/bkcs.2012.33.12.4180