methyl ((1S)-2-(((1R,5S)-1-cyclopropyl-6-hydroxy-5-((3-methylbutyl)(4-nitrophenylsulfonyl)amino)hexyl)amino)-1-diphenylmethyl-2-oxoethyl)carbamate

Base Information

• Chemical Name: methyl ((1S)-2-(((1R,5S)-1-cyclopropyl-6-hydroxy-5-((3-methylbutyl)(4-nitrophenylsulfonyl)amino)hexyl)amino)-1-diphenylmethyl-2-oxoethyl)carbamate
• CAS No.: 1138018-54-8
• Molecular Formula: C₃₇H₄₈N₄O₈S
• Molecular Weight: 708.876

Synonyms:methyl ((1S)-2-(((1R,5S)-1-cyclopropyl-6-hydroxy-5-((3-methylbutyl)(4-nitrophenylsulfonyl)amino)hexyl)amino)-1-diphenylmethyl-2-oxoethyl)carbamate

Chemical Property of methyl ((1S)-2-(((1R,5S)-1-cyclopropyl-6-hydroxy-5-((3-methylbutyl)(4-nitrophenylsulfonyl)amino)hexyl)amino)-1-diphenylmethyl-2-oxoethyl)carbamate

Chemical Property:

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Technology Process of methyl ((1S)-2-(((1R,5S)-1-cyclopropyl-6-hydroxy-5-((3-methylbutyl)(4-nitrophenylsulfonyl)amino)hexyl)amino)-1-diphenylmethyl-2-oxoethyl)carbamate

There total 1 articles about methyl ((1S)-2-(((1R,5S)-1-cyclopropyl-6-hydroxy-5-((3-methylbutyl)(4-nitrophenylsulfonyl)amino)hexyl)amino)-1-diphenylmethyl-2-oxoethyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl ((1S)-2-(((1R,5S)-1-cyclopropyl-6-hydroxy-5-((3-methylbutyl)amino)hexyl)amino)-1-diphenylmethyl-2-oxoethyl)carbamate hydrochloride (1138018-53-7) + 4-Nitrobenzenesulfonyl chloride (98-74-8) → methyl ((1S)-2-(((1R,5S)-1-cyclopropyl-6-hydroxy-5-((3-methylbutyl)(4-nitrophenylsulfonyl)amino)hexyl)amino)-1-diphenylmethyl-2-oxoethyl)carbamate (1138018-54-8)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 19.5h;

Reference yield:

methyl ((1S)-2-(((1R,5S)-1-cyclopropyl-6-hydroxy-5-((3-methylbutyl)(4-nitrophenylsulfonyl)amino)hexyl)amino)-1-diphenylmethyl-2-oxoethyl)carbamate (1138018-54-8) → methyl ((1S)-2-(((1R,5S)-1-cyclopropyl-6-hydroxy-5-((3-methylbutyl)(4-aminophenylsulfonyl)amino)hexyl)amino)-1-diphenylmethyl-2-oxoethyl)carbamate (1138017-82-9)

Guidance literature:

With tin(ll) chloride; In tetrahydrofuran; ethanol; at 85 ℃; for 2.5h;

upstream raw materials:

methyl ((1S)-2-(((1R,5S)-1-cyclopropyl-6-hydroxy-5-((3-methylbutyl)amino)hexyl)amino)-1-diphenylmethyl-2-oxoethyl)carbamate hydrochloride

4-Nitrobenzenesulfonyl chloride

Downstream raw materials:

methyl ((1S)-2-(((1R,5S)-1-cyclopropyl-6-hydroxy-5-((3-methylbutyl)(4-aminophenylsulfonyl)amino)hexyl)amino)-1-diphenylmethyl-2-oxoethyl)carbamate

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