3,3-di(ethoxycarbonyl)-2-(3,4-dimethoxyphenyl)-6,7-dimethoxy-1-tetralone

Base Information

Chemical Name:3,3-di(ethoxycarbonyl)-2-(3,4-dimethoxyphenyl)-6,7-dimethoxy-1-tetralone
CAS No.:114855-46-8
Molecular Formula:C₂₆H₃₀O₉
Molecular Weight:486.519
Hs Code.:

Synonyms:3,3-di(ethoxycarbonyl)-2-(3,4-dimethoxyphenyl)-6,7-dimethoxy-1-tetralone

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Chemical Property of 3,3-di(ethoxycarbonyl)-2-(3,4-dimethoxyphenyl)-6,7-dimethoxy-1-tetralone

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Technology Process of 3,3-di(ethoxycarbonyl)-2-(3,4-dimethoxyphenyl)-6,7-dimethoxy-1-tetralone

There total 1 articles about 3,3-di(ethoxycarbonyl)-2-(3,4-dimethoxyphenyl)-6,7-dimethoxy-1-tetralone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 114855-48-0
triethyl 1,3-bis(3,4-dimethoxyphenyl)propane-1,2,2-tricarboxylate

: 114855-46-8
3,3-di(ethoxycarbonyl)-2-(3,4-dimethoxyphenyl)-6,7-dimethoxy-1-tetralone

Guidance literature:: With boron trifluoride diethyl etherate; In acetic acid; for 15h; Heating; oth. reagents and solvents;

Reference yield: 82.0%

: 593-56-6
N-methoxylamine hydrochloride

: 114855-46-8
3,3-di(ethoxycarbonyl)-2-(3,4-dimethoxyphenyl)-6,7-dimethoxy-1-tetralone

: 128134-23-6
diethyl 4-methoxyimino-3-(3,4-dimethoxyphenyl)-6,7-dimethoxytetralin-2,2-dicarboxylate

Guidance literature:: With pyridine; for 50h; Heating;

Reference yield:

: 114855-46-8
3,3-di(ethoxycarbonyl)-2-(3,4-dimethoxyphenyl)-6,7-dimethoxy-1-tetralone

: 128134-24-7
diethyl 3-(3,4-dimethoxyphenyl)-7,8-dimethoxy-2,3,4,5-tetrahydro-1H-benzoazepin-1-one-4,4-dicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / pyridine / 50 h / Heating

2: 40 percent / stannous chloride / acetic anhydride / 3 h / 100 °C

With pyridine; tin(ll) chloride; In acetic anhydride;