N^η-Z-2,8-diaminooctanoic acid

Base Information

Chemical Name:N^η-Z-2,8-diaminooctanoic acid
CAS No.:101947-55-1
Molecular Formula:C₁₆H₂₄N₂O₄
Molecular Weight:308.378
Hs Code.:

N<sup>η</sup>-Z-2,8-diaminooctanoic acid

Synonyms:N^η-Z-2,8-diaminooctanoic acid

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Chemical Property of N^η-Z-2,8-diaminooctanoic acid

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Technology Process of N^η-Z-2,8-diaminooctanoic acid

There total 5 articles about N^η-Z-2,8-diaminooctanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 63945-11-9
6-phthalimido-1-hexanol

: 101947-55-1
N^η-Z-2,8-diaminooctanoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 68.1 g / PBr₃ / toluene / 100 °C

2: 74 percent / 1.) NaH / 1.) DMF, 10 deg C -> RT, 45 min, 2.) RT, 24 h

3: 91 percent / 6N HCl / 5 h / Heating

4: 1.) CuCl₂, NaOH, 3.) thioacetamide, 2N NaOH / 1.) H₂O, pH 9.5, 2.) 0 deg C, 3.5 h, 3.) pH 8, RT, 24 h

With hydrogenchloride; sodium hydroxide; phosphorus tribromide; sodium hydride; thioacetamide; copper dichloride; In toluene;

Reference yield:

: 4048-33-3
6-amino-1-hexanol

: 101947-55-1
N^η-Z-2,8-diaminooctanoic acid

Guidance literature:: Multi-step reaction with 5 steps

1: toluene / Heating

2: 68.1 g / PBr₃ / toluene / 100 °C

3: 74 percent / 1.) NaH / 1.) DMF, 10 deg C -> RT, 45 min, 2.) RT, 24 h

4: 91 percent / 6N HCl / 5 h / Heating

5: 1.) CuCl₂, NaOH, 3.) thioacetamide, 2N NaOH / 1.) H₂O, pH 9.5, 2.) 0 deg C, 3.5 h, 3.) pH 8, RT, 24 h

With hydrogenchloride; sodium hydroxide; phosphorus tribromide; sodium hydride; thioacetamide; copper dichloride; In toluene;

Reference yield:

: 24566-79-8
2-(6-bromohexyl)isoindole-1,3-dione

: 101947-55-1
N^η-Z-2,8-diaminooctanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 74 percent / 1.) NaH / 1.) DMF, 10 deg C -> RT, 45 min, 2.) RT, 24 h

2: 91 percent / 6N HCl / 5 h / Heating

3: 1.) CuCl₂, NaOH, 3.) thioacetamide, 2N NaOH / 1.) H₂O, pH 9.5, 2.) 0 deg C, 3.5 h, 3.) pH 8, RT, 24 h

With hydrogenchloride; sodium hydroxide; sodium hydride; thioacetamide; copper dichloride;