Technology Process of C33H26N4
There total 3 articles about C33H26N4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
p-(p-tolyl)benzonitrile;
With
sodium azide; tributyltin chloride;
In
toluene;
at 115 ℃;
for 70h;
Inert atmosphere;
trityl chloride;
With
sodium hydroxide;
In
water; toluene;
at 20 ℃;
for 3h;
DOI:10.1016/j.bmc.2013.01.067
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: bis-triphenylphosphine-palladium(II) chloride; lithium chloride / N,N-dimethyl-formamide / Inert atmosphere
2.1: sodium azide; tributyltin chloride / toluene / 70 h / 115 °C / Inert atmosphere
2.2: 3 h / 20 °C
With
bis-triphenylphosphine-palladium(II) chloride; sodium azide; tributyltin chloride; lithium chloride;
In
N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.bmc.2013.01.067
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: bis-triphenylphosphine-palladium(II) chloride; lithium chloride / N,N-dimethyl-formamide / Inert atmosphere
2.1: sodium azide; tributyltin chloride / toluene / 70 h / 115 °C / Inert atmosphere
2.2: 3 h / 20 °C
With
bis-triphenylphosphine-palladium(II) chloride; sodium azide; tributyltin chloride; lithium chloride;
In
N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.bmc.2013.01.067
