benzyl 5,5-dimethyl-2-(methylsulfonyl)-5H-pyrrolo[3,4-d]pyrimidine-6(7H)-carboxylate

Base Information

Chemical Name:benzyl 5,5-dimethyl-2-(methylsulfonyl)-5H-pyrrolo[3,4-d]pyrimidine-6(7H)-carboxylate
CAS No.:1584148-62-8
Molecular Formula:C₁₇H₁₉N₃O₄S
Molecular Weight:361.422
Hs Code.:

Synonyms:benzyl 5,5-dimethyl-2-(methylsulfonyl)-5H-pyrrolo[3,4-d]pyrimidine-6(7H)-carboxylate

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Chemical Property of benzyl 5,5-dimethyl-2-(methylsulfonyl)-5H-pyrrolo[3,4-d]pyrimidine-6(7H)-carboxylate

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Technology Process of benzyl 5,5-dimethyl-2-(methylsulfonyl)-5H-pyrrolo[3,4-d]pyrimidine-6(7H)-carboxylate

There total 7 articles about benzyl 5,5-dimethyl-2-(methylsulfonyl)-5H-pyrrolo[3,4-d]pyrimidine-6(7H)-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 625-05-8
3-amino-3-methylbutanoic acid

: 1584148-62-8
benzyl 5,5-dimethyl-2-(methylsulfonyl)-5H-pyrrolo[3,4-d]pyrimidine-6(7H)-carboxylate

Guidance literature:: Multi-step reaction with 8 steps

1: chloro-trimethyl-silane / 20 °C

2: N-ethyl-N,N-diisopropylamine / acetonitrile; tetrahydrofuran / 20 h / 0 - 20 °C

3: sodium hydrogencarbonate / tetrahydrofuran; water / 0 - 20 °C

4: potassium tert-butylate / toluene / 3 h / -10 - 20 °C

5: N,N-dimethyl acetamide / 1 h / 80 °C

6: potassium acetate / N,N-dimethyl-formamide / 2 h / 90 °C

7: sodium hydroxide / water; 1,4-dioxane / 3 h / 110 °C

8: oxone||potassium monopersulfate triple salt / N,N-dimethyl-formamide / 20 °C

With chloro-trimethyl-silane; oxone||potassium monopersulfate triple salt; potassium tert-butylate; potassium acetate; sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; N,N-dimethyl acetamide; water; N,N-dimethyl-formamide; toluene; acetonitrile;

Reference yield:

: 1584148-41-3
methyl 3-(((benzyloxy)carbonyl)(2-methoxy-2-oxoethyl)amino)-3-methylbutanoate

: 1584148-62-8
benzyl 5,5-dimethyl-2-(methylsulfonyl)-5H-pyrrolo[3,4-d]pyrimidine-6(7H)-carboxylate

Guidance literature:: Multi-step reaction with 5 steps

1: potassium tert-butylate / toluene / 3 h / -10 - 20 °C

2: N,N-dimethyl acetamide / 1 h / 80 °C

3: potassium acetate / N,N-dimethyl-formamide / 2 h / 90 °C

4: sodium hydroxide / water; 1,4-dioxane / 3 h / 110 °C

5: oxone||potassium monopersulfate triple salt / N,N-dimethyl-formamide / 20 °C

With oxone||potassium monopersulfate triple salt; potassium tert-butylate; potassium acetate; sodium hydroxide; In 1,4-dioxane; N,N-dimethyl acetamide; water; N,N-dimethyl-formamide; toluene;

Reference yield:

: 1584148-47-9
6-benzyl 7-methyl 5,5-dimethyl-2-(methylthio)-5H-pyrrolo[3,4-d]pyrimidine-6,7(7H)-dicarboxylate

: 1584148-62-8
benzyl 5,5-dimethyl-2-(methylsulfonyl)-5H-pyrrolo[3,4-d]pyrimidine-6(7H)-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide / water; 1,4-dioxane / 3 h / 110 °C

2: oxone||potassium monopersulfate triple salt / N,N-dimethyl-formamide / 20 °C

With oxone||potassium monopersulfate triple salt; sodium hydroxide; In 1,4-dioxane; water; N,N-dimethyl-formamide;