6-{[4-(4-Hydroxy-benzenesulfonyl)-benzyl]-methyl-amino}-1H-benzo[cd]indol-2-one

Base Information

Chemical Name:6-{[4-(4-Hydroxy-benzenesulfonyl)-benzyl]-methyl-amino}-1H-benzo[cd]indol-2-one
CAS No.:138384-62-0
Molecular Formula:C₂₅H₂₀N₂O₄S
Molecular Weight:444.511
Hs Code.:

Synonyms:6-{[4-(4-Hydroxy-benzenesulfonyl)-benzyl]-methyl-amino}-1H-benzo[cd]indol-2-one

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Chemical Property of 6-{[4-(4-Hydroxy-benzenesulfonyl)-benzyl]-methyl-amino}-1H-benzo[cd]indol-2-one

Chemical Property:

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Technology Process of 6-{[4-(4-Hydroxy-benzenesulfonyl)-benzyl]-methyl-amino}-1H-benzo[cd]indol-2-one

There total 9 articles about 6-{[4-(4-Hydroxy-benzenesulfonyl)-benzyl]-methyl-amino}-1H-benzo[cd]indol-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 130-00-7
1,8-naphtholactam

: 138384-62-0
6-{[4-(4-Hydroxy-benzenesulfonyl)-benzyl]-methyl-amino}-1H-benzo[cd]indol-2-one

Guidance literature:: Multi-step reaction with 4 steps

1: 51 percent / 70percent HNO₃ / acetic acid / 1 h / 20 - 50 °C

2: H₂ / 5percent Pd/C / tetrahydrofuran / 16 h / 2068.6 Torr

3: DIEA / dimethylformamide

4: DIEA / dimethylformamide

With hydrogen; nitric acid; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In tetrahydrofuran; acetic acid; N,N-dimethyl-formamide;
DOI:10.1021/jm00082a006

Reference yield:

: 65300-66-5
N-(2,4-dinitrophenoxy)-4-nitronaphthalimide

: 138384-62-0
6-{[4-(4-Hydroxy-benzenesulfonyl)-benzyl]-methyl-amino}-1H-benzo[cd]indol-2-one

Guidance literature:: Multi-step reaction with 4 steps

1: NaOH / ethanol; H₂O / 16 h / 25 °C

2: H₂ / 5percent Pd/C / tetrahydrofuran / 16 h / 2068.6 Torr

3: DIEA / dimethylformamide

4: DIEA / dimethylformamide

With sodium hydroxide; hydrogen; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In tetrahydrofuran; ethanol; water; N,N-dimethyl-formamide;
DOI:10.1021/jm00082a006

Reference yield:

: 28434-96-0
N-hydroxy-4-nitro-1,8-naphthalimide

: 138384-62-0
6-{[4-(4-Hydroxy-benzenesulfonyl)-benzyl]-methyl-amino}-1H-benzo[cd]indol-2-one

Guidance literature:: Multi-step reaction with 5 steps

1: Na₂CO₃ / H₂O / 1 h / Heating

2: NaOH / ethanol; H₂O / 16 h / 25 °C

3: H₂ / 5percent Pd/C / tetrahydrofuran / 16 h / 2068.6 Torr

4: DIEA / dimethylformamide

5: DIEA / dimethylformamide

With sodium hydroxide; hydrogen; sodium carbonate; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In tetrahydrofuran; ethanol; water; N,N-dimethyl-formamide;
DOI:10.1021/jm00082a006