6,7-anhydro-2-deoxy-3,4,5-tri-O-benzyl-2-trifluoracetamido-D-gluco-D-glycero-hepose-1,1-trimethylene dithioacetal

Base Information

Chemical Name:6,7-anhydro-2-deoxy-3,4,5-tri-O-benzyl-2-trifluoracetamido-D-gluco-D-glycero-hepose-1,1-trimethylene dithioacetal
CAS No.:959409-91-7
Molecular Formula:C₃₃H₃₆F₃NO₅S₂
Molecular Weight:647.78
Hs Code.:

Synonyms:6,7-anhydro-2-deoxy-3,4,5-tri-O-benzyl-2-trifluoracetamido-D-gluco-D-glycero-hepose-1,1-trimethylene dithioacetal

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Chemical Property of 6,7-anhydro-2-deoxy-3,4,5-tri-O-benzyl-2-trifluoracetamido-D-gluco-D-glycero-hepose-1,1-trimethylene dithioacetal

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Technology Process of 6,7-anhydro-2-deoxy-3,4,5-tri-O-benzyl-2-trifluoracetamido-D-gluco-D-glycero-hepose-1,1-trimethylene dithioacetal

There total 1 articles about 6,7-anhydro-2-deoxy-3,4,5-tri-O-benzyl-2-trifluoracetamido-D-gluco-D-glycero-hepose-1,1-trimethylene dithioacetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 959409-89-3
2-deoxy-3,4,5-tri-O-benzyl-2-trifluoracetamido-D-gluco-hexodialdose-1,1-trimethylene dithioacetal

: 1774-47-6
trimethylsulfoxonium iodide

: 959409-91-7
6,7-anhydro-2-deoxy-3,4,5-tri-O-benzyl-2-trifluoracetamido-D-gluco-D-glycero-hepose-1,1-trimethylene dithioacetal

Guidance literature:: trimethylsulfoxonium iodide; With sodium hydride; In dimethyl sulfoxide; at 20 ℃; for 1h;

2-deoxy-3,4,5-tri-O-benzyl-2-trifluoracetamido-D-gluco-hexodialdose-1,1-trimethylene dithioacetal; In dimethyl sulfoxide; at 20 ℃; for 1h; Further stages.;
DOI:10.1039/b711112f

Reference yield: 54.0%

: 959409-91-7
6,7-anhydro-2-deoxy-3,4,5-tri-O-benzyl-2-trifluoracetamido-D-gluco-D-glycero-hepose-1,1-trimethylene dithioacetal

: 959409-94-0
(2R,3R,4R,5R,6S)-3,4,5-tris(benzyloxy)-6-hydroxymethyl-2-trifluoracetamido-cyclohexanone trimethylene dithioacetal

: 959409-95-1
(2R,3R,4S,5R,6R)-3,4,5-tris(benzyloxy)-6-hydroxy-2-trifluoroacetamido-cycloheptanone trimethylene dithioacetal

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane; at -90 - -10 ℃; for 3h; Further Variations:; Reagents; Solvents; Temperatures; reaction time; Product distribution;
DOI:10.1039/b711112f