2-deoxy-3,4,5-tri-O-benzyl-2-trifluoracetamido-D-gluco-hexodialdose-1,1-trimethylene dithioacetal

Base Information

Chemical Name:2-deoxy-3,4,5-tri-O-benzyl-2-trifluoracetamido-D-gluco-hexodialdose-1,1-trimethylene dithioacetal
CAS No.:959409-89-3
Molecular Formula:C₃₂H₃₄F₃NO₅S₂
Molecular Weight:633.753
Hs Code.:

Synonyms:2-deoxy-3,4,5-tri-O-benzyl-2-trifluoracetamido-D-gluco-hexodialdose-1,1-trimethylene dithioacetal

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Chemical Property of 2-deoxy-3,4,5-tri-O-benzyl-2-trifluoracetamido-D-gluco-hexodialdose-1,1-trimethylene dithioacetal

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Technology Process of 2-deoxy-3,4,5-tri-O-benzyl-2-trifluoracetamido-D-gluco-hexodialdose-1,1-trimethylene dithioacetal

There total 1 articles about 2-deoxy-3,4,5-tri-O-benzyl-2-trifluoracetamido-D-gluco-hexodialdose-1,1-trimethylene dithioacetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 959409-88-2
2-deoxy-3,4,5-tri-O-benzyl-2-trifluoracetamido-D-glucose-1,1-trimethylene dithioacetal

: 959409-89-3
2-deoxy-3,4,5-tri-O-benzyl-2-trifluoracetamido-D-gluco-hexodialdose-1,1-trimethylene dithioacetal

Guidance literature:: With Dess-Martin periodane; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1039/b711112f

Reference yield: 61.0%

: 959409-89-3
2-deoxy-3,4,5-tri-O-benzyl-2-trifluoracetamido-D-gluco-hexodialdose-1,1-trimethylene dithioacetal

: 1774-47-6
trimethylsulfoxonium iodide

: 959409-91-7
6,7-anhydro-2-deoxy-3,4,5-tri-O-benzyl-2-trifluoracetamido-D-gluco-D-glycero-hepose-1,1-trimethylene dithioacetal

Guidance literature:: trimethylsulfoxonium iodide; With sodium hydride; In dimethyl sulfoxide; at 20 ℃; for 1h;

2-deoxy-3,4,5-tri-O-benzyl-2-trifluoracetamido-D-gluco-hexodialdose-1,1-trimethylene dithioacetal; In dimethyl sulfoxide; at 20 ℃; for 1h; Further stages.;
DOI:10.1039/b711112f