IC-163

Base Information

• Chemical Name: IC-163
• CAS No.: 521-45-9
• Molecular Formula: C₂₁H₂₂O₇
• Molecular Weight: 386.401

Synonyms:IC-163

Chemical Property of IC-163

Chemical Property:

Purity/Quality:

99%, ^*data from raw suppliers

Wushanicaritin 98.11% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of IC-163

There total 1 articles about IC-163 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ icaritin (118525-40-9) + IC-163 (521-45-9)

Guidance literature:

With potassium hydroxide;

Reference yield: 58.0%

IC-163 (521-45-9) + chloroacetonitrile (107-14-2) → 2-chloro-N-(4-(3,5,7-trihydroxy-2-(4-methoxyphenyl)-4-oxo-4H-chromen-8-yl)-2-methylbutan-2-yl)acetamide (1192136-05-2)

Guidance literature:

With sulfuric acid; acetic acid; at -15 - 20 ℃;

Reference yield:

IC-163 (521-45-9) → 8-(3-amino-3-methylbutyl)-3,5,7-trihydroxy-2-(4-methoxyphenyl)-4H-chromen-4-one (1192135-62-8)

Guidance literature:

Multi-step reaction with 2 steps

1: sulfuric acid; acetic acid / -15 - 20 °C

2: thiourea; acetic acid / ethanol / 50 h / Reflux

With sulfuric acid; acetic acid; thiourea; In ethanol;

Downstream raw materials:

5-hydroxy-8-(3-hydroxy-3-methyl-butyl)-3,7-dimethoxy-2-(4-methoxy-phenyl)-chromen-4-one

2-chloro-N-(4-(3,5,7-trihydroxy-2-(4-methoxyphenyl)-4-oxo-4H-chromen-8-yl)-2-methylbutan-2-yl)acetamide

8-(3-amino-3-methylbutyl)-3,5,7-trihydroxy-2-(4-methoxyphenyl)-4H-chromen-4-one

8-(3-amino-3-methylbutyl)-3,5,7-trihydroxy-2-(4-methoxyphenyl)-4H-chromen-4-one hydrochloride

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