2',3',4',2'',6''-penta-O-acetyl-tetra-N-tert.-butyloxycarbonyl-4''-deoxy-4''-eno-kanamycin A

Base Information

Chemical Name:2',3',4',2'',6''-penta-O-acetyl-tetra-N-tert.-butyloxycarbonyl-4''-deoxy-4''-eno-kanamycin A
CAS No.:83480-09-5
Molecular Formula:C₄₈H₇₆N₄O₂₃
Molecular Weight:1077.14
Hs Code.:

Synonyms:2',3',4',2'',6''-penta-O-acetyl-tetra-N-tert.-butyloxycarbonyl-4''-deoxy-4''-eno-kanamycin A

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Chemical Property of 2',3',4',2'',6''-penta-O-acetyl-tetra-N-tert.-butyloxycarbonyl-4''-deoxy-4''-eno-kanamycin A

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Technology Process of 2',3',4',2'',6''-penta-O-acetyl-tetra-N-tert.-butyloxycarbonyl-4''-deoxy-4''-eno-kanamycin A

There total 8 articles about 2',3',4',2'',6''-penta-O-acetyl-tetra-N-tert.-butyloxycarbonyl-4''-deoxy-4''-eno-kanamycin A which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 83480-05-1,92692-65-4
2',3',4',2,6-penta-O-acetyl-tetra-N-tert.-butyloxycarbonyl-kanamycin A

: 83480-09-5
2',3',4',2'',6''-penta-O-acetyl-tetra-N-tert.-butyloxycarbonyl-4''-deoxy-4''-eno-kanamycin A

Guidance literature:: Multi-step reaction with 4 steps

1: CH₂Cl₂; pyridine / 1 h / -5 °C

2: sodium nitrile / dimethylformamide / 3 h / Ambient temperature

3: CH₂Cl₂; pyridine / 1 h / -5 °C

4: tetrabutylammonium bromide / acetonitrile / 0.5 h / Ambient temperature

With sodium nitrile; tetrabutylammomium bromide; In pyridine; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/0008-6215(84)85075-2

Reference yield:

: 83480-05-1,92692-65-4
2',3',4',2'',6''-penta-O-acethyl-tetra-N-(tert-butoxycaebonyl)-4''-epi-kanamycin A

: 83480-09-5
2',3',4',2'',6''-penta-O-acetyl-tetra-N-tert.-butyloxycarbonyl-4''-deoxy-4''-eno-kanamycin A

Guidance literature:: Multi-step reaction with 2 steps

1: CH₂Cl₂; pyridine / 1 h / -5 °C

2: tetrabutylammonium bromide / acetonitrile / 0.5 h / Ambient temperature

With tetrabutylammomium bromide; In pyridine; dichloromethane; acetonitrile;
DOI:10.1016/0008-6215(84)85075-2

Reference yield:

: 86447-75-8,92692-67-6
C₄₉H₇₇F₃N₄O₂₆S

: 83480-09-5
2',3',4',2'',6''-penta-O-acetyl-tetra-N-tert.-butyloxycarbonyl-4''-deoxy-4''-eno-kanamycin A

Guidance literature:: Multi-step reaction with 3 steps

1: sodium nitrile / dimethylformamide / 3 h / Ambient temperature

2: CH₂Cl₂; pyridine / 1 h / -5 °C

3: tetrabutylammonium bromide / acetonitrile / 0.5 h / Ambient temperature

With sodium nitrile; tetrabutylammomium bromide; In pyridine; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/0008-6215(84)85075-2