2',3',4',2'',6''-penta-O-acetyl-tetra-N-tert.-butyloxycarbonyl-4''-deoxy-4''-epi-iodo-kanamycin A

Base Information

Chemical Name:2',3',4',2'',6''-penta-O-acetyl-tetra-N-tert.-butyloxycarbonyl-4''-deoxy-4''-epi-iodo-kanamycin A
CAS No.:83467-52-1
Molecular Formula:C₄₈H₇₇IN₄O₂₃
Molecular Weight:1205.06
Hs Code.:

Synonyms:2',3',4',2'',6''-penta-O-acetyl-tetra-N-tert.-butyloxycarbonyl-4''-deoxy-4''-epi-iodo-kanamycin A

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Chemical Property of 2',3',4',2'',6''-penta-O-acetyl-tetra-N-tert.-butyloxycarbonyl-4''-deoxy-4''-epi-iodo-kanamycin A

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Technology Process of 2',3',4',2'',6''-penta-O-acetyl-tetra-N-tert.-butyloxycarbonyl-4''-deoxy-4''-epi-iodo-kanamycin A

There total 1 articles about 2',3',4',2'',6''-penta-O-acetyl-tetra-N-tert.-butyloxycarbonyl-4''-deoxy-4''-epi-iodo-kanamycin A which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 83480-05-1,92692-65-4
2',3',4',2,6-penta-O-acetyl-tetra-N-tert.-butyloxycarbonyl-kanamycin A

: 83467-52-1
2',3',4',2'',6''-penta-O-acetyl-tetra-N-tert.-butyloxycarbonyl-4''-deoxy-4''-epi-iodo-kanamycin A

Guidance literature:: With triphenyl phosphite; methyl iodide;
DOI:10.1016/S0040-4039(00)87419-5

Reference yield: 95.0%

: 83467-52-1
2',3',4',2'',6''-penta-O-acetyl-tetra-N-tert.-butyloxycarbonyl-4''-deoxy-4''-epi-iodo-kanamycin A

: 83467-53-2
2',3',4',2'',6''-penta-O-acetyl-tetra-N-tert.-butyloxycarbonyl-4''-deoxy-kanamycin A

Guidance literature:: With hydrogen; triethylamine; Raney nickel (Fluka 83440); In ethanol;
DOI:10.1016/S0040-4039(00)87419-5

Reference yield:

: 83467-52-1
2',3',4',2'',6''-penta-O-acetyl-tetra-N-tert.-butyloxycarbonyl-4''-deoxy-4''-epi-iodo-kanamycin A

: 83480-08-4,96444-03-0
4-Desoxykanamycin A

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / H₂, triethyl amine / Raney nickel (Fluka 83440) / ethanol

2: 2.) trifluoroacetic acid / 1.) Zemplen de-O-acetylation

With hydrogen; triethylamine; trifluoroacetic acid; Raney nickel (Fluka 83440); In ethanol;
DOI:10.1016/S0040-4039(00)87419-5