3-benzoyl-1-(2,2-dicyano-1-cyclopropylvinyl)-2-phenyl-6-cyano-1,2-trans-2,3-trans-1,9-trans-1,2,3,9-tetrahydroindolizine

Base Information

Chemical Name:3-benzoyl-1-(2,2-dicyano-1-cyclopropylvinyl)-2-phenyl-6-cyano-1,2-trans-2,3-trans-1,9-trans-1,2,3,9-tetrahydroindolizine
CAS No.:131003-93-5
Molecular Formula:C₂₉H₂₂N₄O
Molecular Weight:442.52
Hs Code.:

Synonyms:3-benzoyl-1-(2,2-dicyano-1-cyclopropylvinyl)-2-phenyl-6-cyano-1,2-trans-2,3-trans-1,9-trans-1,2,3,9-tetrahydroindolizine

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Chemical Property of 3-benzoyl-1-(2,2-dicyano-1-cyclopropylvinyl)-2-phenyl-6-cyano-1,2-trans-2,3-trans-1,9-trans-1,2,3,9-tetrahydroindolizine

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Technology Process of 3-benzoyl-1-(2,2-dicyano-1-cyclopropylvinyl)-2-phenyl-6-cyano-1,2-trans-2,3-trans-1,9-trans-1,2,3,9-tetrahydroindolizine

There total 4 articles about 3-benzoyl-1-(2,2-dicyano-1-cyclopropylvinyl)-2-phenyl-6-cyano-1,2-trans-2,3-trans-1,9-trans-1,2,3,9-tetrahydroindolizine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 25357-46-4
N-Phenacyl-3-cyanopyridiniumbromid

: 131003-89-9
1,1-dicyano-2-cyclopropyl-4-phenyl-1,3-butadiene

: 131003-93-5
3-benzoyl-1-(2,2-dicyano-1-cyclopropylvinyl)-2-phenyl-6-cyano-1,2-trans-2,3-trans-1,9-trans-1,2,3,9-tetrahydroindolizine

Guidance literature:: With triethylamine; In ethanol; at 20 ℃; for 8h;

Reference yield:

: 17407-30-6
2-(1-cyclopropylethylidene)malononitrile

: 131003-93-5
3-benzoyl-1-(2,2-dicyano-1-cyclopropylvinyl)-2-phenyl-6-cyano-1,2-trans-2,3-trans-1,9-trans-1,2,3,9-tetrahydroindolizine

Guidance literature:: Multi-step reaction with 2 steps

1: 68 percent / triethylamine / propan-2-ol / 0.5 h / Heating

2: 95 percent / triethylamine / methanol / 20 °C

With triethylamine; In methanol; isopropyl alcohol;
DOI:10.1007/BF00486803

Reference yield:

: 100-52-7
benzaldehyde

: 131003-93-5
3-benzoyl-1-(2,2-dicyano-1-cyclopropylvinyl)-2-phenyl-6-cyano-1,2-trans-2,3-trans-1,9-trans-1,2,3,9-tetrahydroindolizine

Guidance literature:: Multi-step reaction with 2 steps

1: 68 percent / triethylamine / propan-2-ol / 0.5 h / Heating

2: 95 percent / triethylamine / methanol / 20 °C

With triethylamine; In methanol; isopropyl alcohol;
DOI:10.1007/BF00486803