chloro[meso-tetrakis(p-trifluoromethylphenyl)porphyrinato]iron(III)

Base Information

Chemical Name:chloro[meso-tetrakis(p-trifluoromethylphenyl)porphyrinato]iron(III)
CAS No.:101954-97-6
Molecular Formula:C₄₈H₂₄ClF₁₂FeN₄
Molecular Weight:976.026
Hs Code.:

Synonyms:chloro[meso-tetrakis(p-trifluoromethylphenyl)porphyrinato]iron(III)

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Chemical Property of chloro[meso-tetrakis(p-trifluoromethylphenyl)porphyrinato]iron(III)

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Technology Process of chloro[meso-tetrakis(p-trifluoromethylphenyl)porphyrinato]iron(III)

There total 1 articles about chloro[meso-tetrakis(p-trifluoromethylphenyl)porphyrinato]iron(III) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 56420-24-7
5,10,15,20-tetrakis<4-(trifluoromethyl)phenyl>porphyrin

: iron(II) chloride tetrahydrate

: 101954-97-6
chloro[meso-tetrakis(p-trifluoromethylphenyl)porphyrinato]iron(III)

Guidance literature:: In N,N-dimethyl-formamide;
DOI:10.1016/j.poly.2016.08.048

Reference yield: 54.0%

: 101954-97-6
chloro[meso-tetrakis(p-trifluoromethylphenyl)porphyrinato]iron(III)

: 132125-45-2
(TpCF₃PP)Fe(C₆H₅)

Guidance literature:: With phenyl magnesium bromide; In benzene; under Ar using Schlenk techniques, dropwise addn. (via syringe) of phenylMgBr soln. to (TpCF3PP)FeCl soln., hydrolyzation (H2O); org. layer washed (H2O), sepd., filtrated, rapidly chromd. (basic alumina/benzene), evapn. of solvent under reduced pressure, recrystn. (benzene/heptane), elem.anal.;

Reference yield: 45.0%

: 101954-97-6
chloro[meso-tetrakis(p-trifluoromethylphenyl)porphyrinato]iron(III)

: 879-05-0
2,3,4,5,6-pentafluorophenylmagnesium bromide

: 132125-47-4
(TpCF₃PP)Fe(C₆F₅)

Guidance literature:: In benzene; under Ar using Schlenk techniques, dropwise addn. in the dark of C6F5MgBr to (TpCF3PP)FeCl soln., mixt. was allowed to stand for 48 h, hydrolyzation (H2O) until neutrality; dried (MgSO4), filtered, concd. by evapn. under reduced pressure, chromy. in the dark (basic alumina/benzene), recrystn. (toluene/heptane), elem.anal.;