3,6-bis(4-methoxyphenyl)[1,2,4]triazolo[3,4-b][1,3,4]thiadiazole

Base Information

• Chemical Name: 3,6-bis(4-methoxyphenyl)[1,2,4]triazolo[3,4-b][1,3,4]thiadiazole
• CAS No.: 73014-97-8
• Molecular Formula: C₁₇H₁₄N₄O₂S
• Molecular Weight: 338.39
• Mol file: 73014-97-8.mol

Synonyms:6-(4-methoxyphenyl)-3-(4-methoxyphenyl)-1,2,4-triazolo[3,4-b][1,3,4]thiadiazole

Chemical Property of 3,6-bis(4-methoxyphenyl)[1,2,4]triazolo[3,4-b][1,3,4]thiadiazole

Chemical Property:

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Technology Process of 3,6-bis(4-methoxyphenyl)[1,2,4]triazolo[3,4-b][1,3,4]thiadiazole

There total 3 articles about 3,6-bis(4-methoxyphenyl)[1,2,4]triazolo[3,4-b][1,3,4]thiadiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

(Z)-3-chloro-3-(4-methoxyphenyl)acrylic acid (501334-23-2) + 4-amino-5-(4-methoxyphenyl)-4H-1,2,4-triazole-3-thiol (36209-49-1) → 6-(4-methoxyphenyl)-3-(4-methoxyphenyl)-1,2,4-triazolo[3,4-b][1,3,4]thiadiazole (73014-97-8)

Guidance literature:

With trichlorophosphate; at 80 ℃; for 1h;

DOI:10.1016/j.tetlet.2014.05.059

Reference yield: 84.0%

Thiocarbohydrazide (2231-57-4) + 4-methoxybenzoic acid (100-09-4) → 6-(4-methoxyphenyl)-3-(4-methoxyphenyl)-1,2,4-triazolo[3,4-b][1,3,4]thiadiazole (73014-97-8)

Guidance literature:

With silica-supported dichlorophosphate; In ethanol; for 0.133333h; Microwave irradiation; Reflux;

DOI:10.1080/00397910902838912

Reference yield: 58.0%

acetonitrile (75-05-8,26809-02-9) + 2-(4-methoxybenzylidene)-1-(5-(4-methoxyphenyl)-1,3,4-thiadiazol-2-yl)hydrazine → 6-(4-methoxyphenyl)-3-(4-methoxyphenyl)-1,2,4-triazolo[3,4-b][1,3,4]thiadiazole (73014-97-8) + 2-(5-methyl-3-(4-methoxyphenyl)-1H-[1,2,4]triazol-1-yl)-5-(4-methoxyphenyl)-1,3,4-thiadiazole (1304568-28-2)

Guidance literature:

With lithium perchlorate; at 20 ℃; Electrochemical reaction;

DOI:10.1016/j.tet.2011.02.084

upstream raw materials:

Thiocarbohydrazide

4-methoxybenzoic acid

acetonitrile

(Z)-3-chloro-3-(4-methoxyphenyl)acrylic acid

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