(S)-2-glutarsaeure-5-benzyl-1-(tert-butyl)ester

Base Information

Chemical Name:(S)-2-glutarsaeure-5-benzyl-1-(tert-butyl)ester
CAS No.:129241-86-7
Molecular Formula:C₂₆H₃₉NO₈
Molecular Weight:493.598
Hs Code.:

(S)-2-<Bis(tert-butyloxycarbonyl)amino>glutarsaeure-5-benzyl-1-(tert-butyl)ester

Synonyms:(S)-2-glutarsaeure-5-benzyl-1-(tert-butyl)ester

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Chemical Property of (S)-2-glutarsaeure-5-benzyl-1-(tert-butyl)ester

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Technology Process of (S)-2-glutarsaeure-5-benzyl-1-(tert-butyl)ester

There total 6 articles about (S)-2-glutarsaeure-5-benzyl-1-(tert-butyl)ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 28812-54-6
N-tert-butoxyxarbonyl-L-glutamic acid γ-benzyl α-tert-butyl diester

: 129241-86-7
(S)-2-glutarsaeure-5-benzyl-1-(tert-butyl)ester

Guidance literature:: With dmap; In acetonitrile;
DOI:10.1039/a909722h

Reference yield:

: 91229-91-3
tert-butyl (S)-N-tert-butoxycarbonylpyroglutamate

: 129241-86-7
(S)-2-glutarsaeure-5-benzyl-1-(tert-butyl)ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: 96 percent / aq. LiOH / tetrahydrofuran / 0.25 h / 0 °C

2.1: Et₃N / acetone / 1 h / 20 °C

2.2: 67 percent / acetone / 96 h / Heating

3.1: 80 percent / 4-dimethylaminopyridine / acetonitrile / 72 h / 20 °C

With dmap; lithium hydroxide; triethylamine; In tetrahydrofuran; acetone; acetonitrile;
DOI:10.1039/b503900b

Reference yield:

: 24277-39-2
N-tert-butoxycarbonyl glutamic acid tert-butyl ester

: 129241-86-7
(S)-2-glutarsaeure-5-benzyl-1-(tert-butyl)ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: Et₃N / acetone / 1 h / 20 °C

1.2: 67 percent / acetone / 96 h / Heating

2.1: 80 percent / 4-dimethylaminopyridine / acetonitrile / 72 h / 20 °C

With dmap; triethylamine; In acetone; acetonitrile;
DOI:10.1039/b503900b