(Z)-methyl N-2-bromophenylpentanimidate

Base Information

• Chemical Name: (Z)-methyl N-2-bromophenylpentanimidate
• CAS No.: 1402939-15-4
• Molecular Formula: C₁₂H₁₆BrNO
• Molecular Weight: 270.169
• Mol file: 1402939-15-4.mol

Synonyms:(Z)-methyl N-2-bromophenylpentanimidate

Chemical Property of (Z)-methyl N-2-bromophenylpentanimidate

Chemical Property:

Purity/Quality:

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Technology Process of (Z)-methyl N-2-bromophenylpentanimidate

There total 1 articles about (Z)-methyl N-2-bromophenylpentanimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

trimethyl orthovalerate (13820-09-2) + 2-bromoaniline (615-36-1) → (Z)-methyl N-2-bromophenylpentanimidate (1402939-15-4)

Guidance literature:

With toluene-4-sulfonic acid; In toluene; for 3h; Inert atmosphere; Reflux;

DOI:10.1021/jo301805d

Reference yield: 94.0%

(Z)-methyl N-2-bromophenylpentanimidate (1402939-15-4) + p-toluidine (106-49-0,12221-03-3) → 2-butyl-1-p-tolyl-1H-benzo[d]imidazole (612049-99-7)

Guidance literature:

With palladium diacetate; sodium t-butanolate; catacxium A; at 150 ℃; for 2h; Inert atmosphere; Microwave irradiation;

DOI:10.1021/jo301805d

Reference yield: 71.0%

(Z)-methyl N-2-bromophenylpentanimidate (1402939-15-4) + p-toluidine (106-49-0,12221-03-3) → 2-butyl-3-(4-tolyl)quinazolin-4(3H)-one (330829-50-0)

Guidance literature:

With carbon monoxide; palladium diacetate; caesium carbonate; catacxium A; In toluene; at 85 ℃; for 18h; Inert atmosphere; Microwave irradiation;

DOI:10.1021/jo301805d

upstream raw materials:

trimethyl orthovalerate

2-bromoaniline

Downstream raw materials:

2-butyl-1-p-tolyl-1H-benzo[d]imidazole

2-butyl-3-(4-tolyl)quinazolin-4(3H)-one