Benzyl (2S)-2-amino-3-(4'-(benzyloxy)-3'-{(2S)-2-{[(benzyloxy)carbonyl]amino}-3-oxo-3-[2-(trimethylsilyl)ethoxy]propyl}-4-fluorobiphenyl-3-yl)propanoate hydrochloride

Base Information

• Chemical Name: Benzyl (2S)-2-amino-3-(4'-(benzyloxy)-3'-{(2S)-2-{[(benzyloxy)carbonyl]amino}-3-oxo-3-[2-(trimethylsilyl)ethoxy]propyl}-4-fluorobiphenyl-3-yl)propanoate hydrochloride
• CAS No.: 856222-61-2
• Molecular Formula: C₄₅H₄₉FN₂O₇Si*ClH
• Molecular Weight: 813.438

Synonyms:Benzyl (2S)-2-amino-3-(4'-(benzyloxy)-3'-{(2S)-2-{[(benzyloxy)carbonyl]amino}-3-oxo-3-[2-(trimethylsilyl)ethoxy]propyl}-4-fluorobiphenyl-3-yl)propanoate hydrochloride

Chemical Property of Benzyl (2S)-2-amino-3-(4'-(benzyloxy)-3'-{(2S)-2-{[(benzyloxy)carbonyl]amino}-3-oxo-3-[2-(trimethylsilyl)ethoxy]propyl}-4-fluorobiphenyl-3-yl)propanoate hydrochloride

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Technology Process of Benzyl (2S)-2-amino-3-(4'-(benzyloxy)-3'-{(2S)-2-{[(benzyloxy)carbonyl]amino}-3-oxo-3-[2-(trimethylsilyl)ethoxy]propyl}-4-fluorobiphenyl-3-yl)propanoate hydrochloride

There total 1 articles about Benzyl (2S)-2-amino-3-(4'-(benzyloxy)-3'-{(2S)-2-{[(benzyloxy)carbonyl]amino}-3-oxo-3-[2-(trimethylsilyl)ethoxy]propyl}-4-fluorobiphenyl-3-yl)propanoate hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

2-trimethylsilyl-ethyl (2S)-3-(3'-{(2S)-3-benzyloxy-2-[(tert-butoxycarbonyl)amino]-3-oxo-propyl}-4'-fluoro-4-hydroxy-biphenyl-3-yl)-2-{[(benzyloxy)carbonyl]amino}-propanoate (856222-50-9) → Benzyl (2S)-2-amino-3-(4'-(benzyloxy)-3'-{(2S)-2-{[(benzyloxy)carbonyl]amino}-3-oxo-3-[2-(trimethylsilyl)ethoxy]propyl}-4-fluorobiphenyl-3-yl)propanoate hydrochloride (856222-61-2)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; at 0 ℃; for 3h;

Reference yield: 75.0%

Benzyl (2S)-2-amino-3-(4'-(benzyloxy)-3'-{(2S)-2-{[(benzyloxy)carbonyl]amino}-3-oxo-3-[2-(trimethylsilyl)ethoxy]propyl}-4-fluorobiphenyl-3-yl)propanoate hydrochloride (856222-61-2) + Boc-Orn(Z)-OH (2480-93-5) → 2-trimethylsilyl-ethyl (2S)-3-{3'-[(2S)-3-benzyloxy-2-({(2S)-5-benzyloxycarbonylamino-2-[(tert-butoxycarbonyl)amino]-pentanoyl}amino)-3-oxo-propyl]-4'-fluoro-4-hydroxy-biphenyl-3-y}-2-{[(benzyloxy)carbonyl]amino}-propanoate (856222-72-5)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; HATU; In N,N-dimethyl-formamide; at 0 - 20 ℃;

upstream raw materials:

2-trimethylsilyl-ethyl (2S)-3-(3'-{(2S)-3-benzyloxy-2-[(tert-butoxycarbonyl)amino]-3-oxo-propyl}-4'-fluoro-4-hydroxy-biphenyl-3-yl)-2-{[(benzyloxy)carbonyl]amino}-propanoate

Downstream raw materials:

2-trimethylsilyl-ethyl (2S)-3-{3'-[(2S)-3-benzyloxy-2-({(2S)-5-benzyloxycarbonylamino-2-[(tert-butoxycarbonyl)amino]-pentanoyl}amino)-3-oxo-propyl]-4'-fluoro-4-hydroxy-biphenyl-3-y}-2-{[(benzyloxy)carbonyl]amino}-propanoate

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