2-bromo-5-tert-butyl-N-(1-chloro-2-methylpropan-2-yl)-3-(4,4-dimethyl-4,5-dihydrooxazol-2-yl)benzamide

Base Information

Chemical Name:2-bromo-5-tert-butyl-N-(1-chloro-2-methylpropan-2-yl)-3-(4,4-dimethyl-4,5-dihydrooxazol-2-yl)benzamide
CAS No.:1315258-26-4
Molecular Formula:C₂₀H₂₈BrClN₂O₂
Molecular Weight:443.812
Hs Code.:

Synonyms:2-bromo-5-tert-butyl-N-(1-chloro-2-methylpropan-2-yl)-3-(4,4-dimethyl-4,5-dihydrooxazol-2-yl)benzamide

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Chemical Property of 2-bromo-5-tert-butyl-N-(1-chloro-2-methylpropan-2-yl)-3-(4,4-dimethyl-4,5-dihydrooxazol-2-yl)benzamide

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Technology Process of 2-bromo-5-tert-butyl-N-(1-chloro-2-methylpropan-2-yl)-3-(4,4-dimethyl-4,5-dihydrooxazol-2-yl)benzamide

There total 3 articles about 2-bromo-5-tert-butyl-N-(1-chloro-2-methylpropan-2-yl)-3-(4,4-dimethyl-4,5-dihydrooxazol-2-yl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₀H₃₁BrN₂O₄

: 1315258-26-4
2-bromo-5-tert-butyl-N-(1-chloro-2-methylpropan-2-yl)-3-(4,4-dimethyl-4,5-dihydrooxazol-2-yl)benzamide

Guidance literature:: With methanesulfonyl chloride; triethylamine; In dichloromethane; at 0 - 20 ℃; for 16h; Inert atmosphere;
DOI:10.1039/c1cc12071a

Reference yield:

: 64395-03-5
2-bromo-5-tert-butyl-isophthalic acid

: 1315258-26-4
2-bromo-5-tert-butyl-N-(1-chloro-2-methylpropan-2-yl)-3-(4,4-dimethyl-4,5-dihydrooxazol-2-yl)benzamide

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride; N,N-dimethyl-formamide / Inert atmosphere

2: triethylamine / dichloromethane / 5 h / 0 - 20 °C / Inert atmosphere

3: methanesulfonyl chloride; triethylamine / dichloromethane / 16 h / 0 - 20 °C / Inert atmosphere

With thionyl chloride; methanesulfonyl chloride; triethylamine; N,N-dimethyl-formamide; In dichloromethane;
DOI:10.1039/c1cc12071a

Reference yield:

: 194734-10-6
2-bromo-5-tert-butylisophthalic acid chloride

: 1315258-26-4
2-bromo-5-tert-butyl-N-(1-chloro-2-methylpropan-2-yl)-3-(4,4-dimethyl-4,5-dihydrooxazol-2-yl)benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 5 h / 0 - 20 °C / Inert atmosphere

2: methanesulfonyl chloride; triethylamine / dichloromethane / 16 h / 0 - 20 °C / Inert atmosphere

With methanesulfonyl chloride; triethylamine; In dichloromethane;
DOI:10.1039/c1cc12071a