Acetic acid (4S,5R)-5-acetoxymethyl-1,3-dibenzyl-2-oxo-imidazolidin-4-ylmethyl ester

Base Information

Chemical Name:Acetic acid (4S,5R)-5-acetoxymethyl-1,3-dibenzyl-2-oxo-imidazolidin-4-ylmethyl ester
CAS No.:95790-94-6
Molecular Formula:C₂₃H₂₆N₂O₅
Molecular Weight:410.47
Hs Code.:

Synonyms:Acetic acid (4S,5R)-5-acetoxymethyl-1,3-dibenzyl-2-oxo-imidazolidin-4-ylmethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Acetic acid (4S,5R)-5-acetoxymethyl-1,3-dibenzyl-2-oxo-imidazolidin-4-ylmethyl ester

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Technology Process of Acetic acid (4S,5R)-5-acetoxymethyl-1,3-dibenzyl-2-oxo-imidazolidin-4-ylmethyl ester

There total 12 articles about Acetic acid (4S,5R)-5-acetoxymethyl-1,3-dibenzyl-2-oxo-imidazolidin-4-ylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 108-24-7
acetic anhydride

: 56198-32-4
cis-1,3-dibenzyl-4,5-dihydroxymethyl-imidazolidin-2-one

: 95790-94-6
Acetic acid (4S,5R)-5-acetoxymethyl-1,3-dibenzyl-2-oxo-imidazolidin-4-ylmethyl ester

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 20 ℃; for 4h; Inert atmosphere;
DOI:10.1016/j.molcatb.2013.09.014

Reference yield: 90.0%

: 108-05-4,9003-20-7
vinyl acetate

: 56198-32-4
cis-1,3-dibenzyl-4,5-dihydroxymethyl-imidazolidin-2-one

: C₂₁H₂₄N₂O₄

: 95790-94-6
Acetic acid (4S,5R)-5-acetoxymethyl-1,3-dibenzyl-2-oxo-imidazolidin-4-ylmethyl ester

Guidance literature:: With Lipozyme RM IM; In 1,4-dioxane; toluene; at 35 ℃; for 6h; Solvent; Reagent/catalyst; Temperature; enantioselective reaction; Enzymatic reaction;
DOI:10.1016/j.molcatb.2013.09.014

Reference yield: 78.96%

: 123-86-4
acetic acid butyl ester

: 56198-32-4
cis-1,3-dibenzyl-4,5-dihydroxymethyl-imidazolidin-2-one

: C₂₁H₂₄N₂O₄

: 95790-94-6
Acetic acid (4S,5R)-5-acetoxymethyl-1,3-dibenzyl-2-oxo-imidazolidin-4-ylmethyl ester

Guidance literature:: With Lipozyme RM IM; In dichloromethane; at 30 ℃; for 24h; enantioselective reaction; Enzymatic reaction;
DOI:10.1016/j.molcatb.2013.09.014