N⁽¹⁾-(4-bromophenyl)-N⁽²⁾,N⁽²⁾-bis(pyridin-2-ylmethyl)ethane-1,2-diamine

Base Information

Chemical Name:N⁽¹⁾-(4-bromophenyl)-N⁽²⁾,N⁽²⁾-bis(pyridin-2-ylmethyl)ethane-1,2-diamine
CAS No.:1489265-48-6
Molecular Formula:C₂₀H₂₁BrN₄
Molecular Weight:397.318
Hs Code.:

N<sup>(1)</sup>-(4-bromophenyl)-N<sup>(2)</sup>,N<sup>(2)</sup>-bis(pyridin-2-ylmethyl)ethane-1,2-diamine

Synonyms:N⁽¹⁾-(4-bromophenyl)-N⁽²⁾,N⁽²⁾-bis(pyridin-2-ylmethyl)ethane-1,2-diamine

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Chemical Property of N⁽¹⁾-(4-bromophenyl)-N⁽²⁾,N⁽²⁾-bis(pyridin-2-ylmethyl)ethane-1,2-diamine

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Technology Process of N⁽¹⁾-(4-bromophenyl)-N⁽²⁾,N⁽²⁾-bis(pyridin-2-ylmethyl)ethane-1,2-diamine

There total 3 articles about N⁽¹⁾-(4-bromophenyl)-N⁽²⁾,N⁽²⁾-bis(pyridin-2-ylmethyl)ethane-1,2-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 6959-47-3
2-chloromethylpyridine hydrochloride

: 50622-52-1
N¹-(4-bromophenyl)ethane-1,2-diamine

: 1489265-48-6
N⁽¹⁾-(4-bromophenyl)-N⁽²⁾,N⁽²⁾-bis(pyridin-2-ylmethyl)ethane-1,2-diamine

Guidance literature:: With N-ethyl-N,N-diisopropylamine; potassium iodide; In acetonitrile; for 12h; Reflux;
DOI:10.1016/j.dyepig.2013.06.027

Reference yield:

: 589-87-7
1,4-bromoiodobenzene

: 1-(3-(N-carbazolyl)biphenyl)lisoquinoline

: 1-(3-(N-(3, 6-dibromocarbazolyl)))biphenylisoquinoline

: 1439984-82-3
(R)-2-(1-(4-bromophenyl)vinyl)tetrahydrofuran

: 960010-51-9
C₁₉H₁₈Br₂O₂

: 131061-14-8,91911-22-7
n-butyl 4-bromocinnamate

: 1489265-48-6
N⁽¹⁾-(4-bromophenyl)-N⁽²⁾,N⁽²⁾-bis(pyridin-2-ylmethyl)ethane-1,2-diamine

Guidance literature:: Multi-step reaction with 3 steps

1: copper(l) chloride; potassium hydroxide; 1,10-Phenanthroline

2: potassium iodide; potassium iodate / acetic acid

3: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide

With bis-triphenylphosphine-palladium(II) chloride; potassium iodate; copper(l) iodide; 1,10-Phenanthroline; potassium iodide; copper(l) chloride; potassium hydroxide; In acetic acid;
DOI:10.1016/j.dyepig.2013.12.016

Reference yield:

: 589-87-7
1,4-bromoiodobenzene

: 1-(3-(N-carbazolyl)biphenyl)lisoquinoline

: 1-(3-(N-(3, 6-dibromocarbazolyl)))biphenylisoquinoline

: 1439984-82-3
(R)-2-(1-(4-bromophenyl)vinyl)tetrahydrofuran

: 960010-51-9
C₁₉H₁₈Br₂O₂

: 131061-14-8,91911-22-7
n-butyl 4-bromocinnamate

: 1489265-48-6
N⁽¹⁾-(4-bromophenyl)-N⁽²⁾,N⁽²⁾-bis(pyridin-2-ylmethyl)ethane-1,2-diamine

: (S)-2-(1-(4-bromophenyl)vinyl)tetrahydrofuran

: 1-(3-(N-carbazolyl)biphenyl)-3, 4-dihydoisoquinoline

Guidance literature:: Multi-step reaction with 3 steps

1: copper(l) chloride; potassium hydroxide; 1,10-Phenanthroline

2: potassium iodide; potassium iodate / acetic acid

3: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide

With bis-triphenylphosphine-palladium(II) chloride; potassium iodate; copper(l) iodide; 1,10-Phenanthroline; potassium iodide; copper(l) chloride; potassium hydroxide; In acetic acid;
DOI:10.1016/j.dyepig.2013.12.016