5-(4-(2-(4-chlorobenzenesulphonylamino)ethyl)phenyl)-5-(3-pyridyl)pentanoic acid

Base Information

Chemical Name:5-(4-(2-(4-chlorobenzenesulphonylamino)ethyl)phenyl)-5-(3-pyridyl)pentanoic acid
CAS No.:133276-62-7
Molecular Formula:C₂₄H₂₅ClN₂O₄S
Molecular Weight:472.993
Hs Code.:

Synonyms:5-(4-(2-(4-chlorobenzenesulphonylamino)ethyl)phenyl)-5-(3-pyridyl)pentanoic acid

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Chemical Property of 5-(4-(2-(4-chlorobenzenesulphonylamino)ethyl)phenyl)-5-(3-pyridyl)pentanoic acid

Chemical Property:

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Technology Process of 5-(4-(2-(4-chlorobenzenesulphonylamino)ethyl)phenyl)-5-(3-pyridyl)pentanoic acid

There total 6 articles about 5-(4-(2-(4-chlorobenzenesulphonylamino)ethyl)phenyl)-5-(3-pyridyl)pentanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 21.0%

: 767254-86-4
5-(4-(2-aminoethyl)phenyl)-5-(3-pyridyl)pentanoic acid

: 98-60-2
4-chlorobenzenesulfonyl chloride

: 133276-62-7
5-(4-(2-(4-chlorobenzenesulphonylamino)ethyl)phenyl)-5-(3-pyridyl)pentanoic acid

Guidance literature:

Reference yield:

: 153732-04-8
(E)-5-[4-(2-{[(4-chlorophenyl)sulfonyl]amino}ethyl)phenyl]-5-(3-pyridyl)pent-4-enoic acid

: 133276-62-7
5-(4-(2-(4-chlorobenzenesulphonylamino)ethyl)phenyl)-5-(3-pyridyl)pentanoic acid

Guidance literature:: With sodium hydroxide; hydrogen; palladium on activated charcoal; at 40 ℃; for 2h; under 3750.3 Torr;

Reference yield:

: 877-95-2
methyl-N-(benzyl-methyl)-formamide

: 133276-62-7
5-(4-(2-(4-chlorobenzenesulphonylamino)ethyl)phenyl)-5-(3-pyridyl)pentanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) AlCl₃, 2.) 6 N aq. HCl, 3.) 10 N NaHCO₃, NaOH

2: 70 percent / potassium tert-butoxide / tetrahydrofuran / 1.5 h / -20 - 10 °C

3: H₂, 0.3 aq. NaOH / 10percent Pd/C / 2 h / 40 °C / 3750.3 Torr

With hydrogenchloride; sodium hydroxide; aluminium trichloride; potassium tert-butylate; hydrogen; sodium hydrogencarbonate; palladium on activated charcoal; In tetrahydrofuran;