(1S,3S,4R,6S)-6-isopropenyl-3,4-dimethyl-2-oxo-1-(3-oxo-butyl)-cyclohexanecarbaldehyde

Base Information

Chemical Name:(1S,3S,4R,6S)-6-isopropenyl-3,4-dimethyl-2-oxo-1-(3-oxo-butyl)-cyclohexanecarbaldehyde
CAS No.:272766-59-3
Molecular Formula:C₁₆H₂₄O₃
Molecular Weight:264.365
Hs Code.:

Synonyms:(1S,3S,4R,6S)-6-isopropenyl-3,4-dimethyl-2-oxo-1-(3-oxo-butyl)-cyclohexanecarbaldehyde

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Chemical Property of (1S,3S,4R,6S)-6-isopropenyl-3,4-dimethyl-2-oxo-1-(3-oxo-butyl)-cyclohexanecarbaldehyde

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Technology Process of (1S,3S,4R,6S)-6-isopropenyl-3,4-dimethyl-2-oxo-1-(3-oxo-butyl)-cyclohexanecarbaldehyde

There total 2 articles about (1S,3S,4R,6S)-6-isopropenyl-3,4-dimethyl-2-oxo-1-(3-oxo-butyl)-cyclohexanecarbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 78-94-4,25038-87-3
methyl vinyl ketone

: 272767-11-0
(3R,5S)-6-hydroxymethylene-5-isopropenyl-2,3-dimethylcyclohexanone

: 272766-59-3
(1S,3S,4R,6S)-6-isopropenyl-3,4-dimethyl-2-oxo-1-(3-oxo-butyl)-cyclohexanecarbaldehyde

Guidance literature:: With potassium hydroxide; triethylamine; In ethyl acetate; at 20 ℃; for 18h;
DOI:10.1016/S0040-4020(00)00110-1

Reference yield:

: 20549-39-7,20549-40-0,50910-65-1,114298-14-5,137766-27-9,137766-28-0
(3R,5R)-5-isopropenyl-3-methyl-2-oxo-3-cyclohexenecarbonitrile

: 272766-59-3
(1S,3S,4R,6S)-6-isopropenyl-3,4-dimethyl-2-oxo-1-(3-oxo-butyl)-cyclohexanecarbaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / NaH / diethyl ether / 20 °C

2: 97 percent / Et₃N; KOH / ethyl acetate / 18 h / 20 °C

With potassium hydroxide; sodium hydride; triethylamine; In diethyl ether; ethyl acetate; 1: Formylation / 2: Michael addition;
DOI:10.1016/S0040-4020(00)00110-1