2-(7-chloro-9-methyl-2-phenyl-9H-pyrimido[4,5-b]indol-4-yl)-N,N-dimethylacetamide

Base Information

Chemical Name:2-(7-chloro-9-methyl-2-phenyl-9H-pyrimido[4,5-b]indol-4-yl)-N,N-dimethylacetamide
CAS No.:913239-78-8
Molecular Formula:C₂₁H₁₉ClN₄O
Molecular Weight:378.861
Hs Code.:

Synonyms:2-(7-chloro-9-methyl-2-phenyl-9H-pyrimido[4,5-b]indol-4-yl)-N,N-dimethylacetamide

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Chemical Property of 2-(7-chloro-9-methyl-2-phenyl-9H-pyrimido[4,5-b]indol-4-yl)-N,N-dimethylacetamide

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Technology Process of 2-(7-chloro-9-methyl-2-phenyl-9H-pyrimido[4,5-b]indol-4-yl)-N,N-dimethylacetamide

There total 2 articles about 2-(7-chloro-9-methyl-2-phenyl-9H-pyrimido[4,5-b]indol-4-yl)-N,N-dimethylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 913240-25-2
ethyl 2-(7-chloro-9-methyl-2-phenyl-9H-pyrimido[4,5-b]indol-4-yl)-3-(dimethylamino)-3-oxopropanoate

: 913239-78-8
2-(7-chloro-9-methyl-2-phenyl-9H-pyrimido[4,5-b]indol-4-yl)-N,N-dimethylacetamide

Guidance literature:: With methanol; lithium hydroxide; water; In tetrahydrofuran; at 50 ℃; for 2h;

Reference yield:

: 913240-24-1
4-bromo-7-chloro-9-methyl-2-phenyl-9H-pyrimido[4,5-b]indole

: 924-61-8
ethyl 3-(dimethylamino)-3-oxopropanoate

: 913239-78-8
2-(7-chloro-9-methyl-2-phenyl-9H-pyrimido[4,5-b]indol-4-yl)-N,N-dimethylacetamide

: 913240-25-2
ethyl 2-(7-chloro-9-methyl-2-phenyl-9H-pyrimido[4,5-b]indol-4-yl)-3-(dimethylamino)-3-oxopropanoate

Guidance literature:: ethyl 3-(dimethylamino)-3-oxopropanoate; With sodium hydride; In 1,4-dioxane; at 0 - 20 ℃; for 0.5h;

4-bromo-7-chloro-9-methyl-2-phenyl-9H-pyrimido[4,5-b]indole; With copper(l) iodide; In 1,4-dioxane; for 20h; Heating / reflux;