trans-[Co(N,N'-bis(2-pyridinecarboxamide)-1,2-benzene dianion)(benzylamine)2][ClO₄]

Base Information

• Chemical Name: trans-[Co(N,N'-bis(2-pyridinecarboxamide)-1,2-benzene dianion)(benzylamine)2][ClO₄]
• CAS No.: 494845-51-1
• Molecular Formula: C₃₂H₃₀CoN₆O₂*ClO₄
• Molecular Weight: 689.073

Synonyms:trans-[Co(N,N'-bis(2-pyridinecarboxamide)-1,2-benzene dianion)(benzylamine)2][ClO₄]

Chemical Property of trans-[Co(N,N'-bis(2-pyridinecarboxamide)-1,2-benzene dianion)(benzylamine)2][ClO₄]

Chemical Property:

Purity/Quality:

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Technology Process of trans-[Co(N,N'-bis(2-pyridinecarboxamide)-1,2-benzene dianion)(benzylamine)2][ClO₄]

There total 1 articles about trans-[Co(N,N'-bis(2-pyridinecarboxamide)-1,2-benzene dianion)(benzylamine)2][ClO₄] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

sodium perchlorate monohydrate (7791-07-3) + [Co(N,N'-bis(2-pyridinecarboxamide)-1,2-benzene dianion)]hydrate (70559-56-7) + benzylamine (100-46-9) → trans-[Co(N,N'-bis(2-pyridinecarboxamide)-1,2-benzene dianion)(benzylamine)2][ClO4] (494845-51-1)

Guidance literature:

With air; In methanol; to soln. of Co-complex in MeOH added dropwise benzylamine; air bubbled for 3 h, MeOH added during this period; mixt. filtered off; soln. of NaClO4*H2O in MeOH added to filtrate; after 48 h crystals filtered; washed (cold EtOH, ether); recrystd. (MeCM/EtOH); crystals collected; washed (cold EtOH, ether); dried (vac.); elem. anal.;

DOI:10.1016/S0020-1693(02)00906-4

upstream raw materials:

sodium perchlorate monohydrate

[Co(N,N'-bis(2-pyridinecarboxamide)-1,2-benzene dianion)]hydrate

benzylamine

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