6-[3,4,5-tris{3-(N-tert-butoxycarbonyl)amino-1-propanoxy}benzoylamino]hexanoic acid

Base Information

• Chemical Name: 6-[3,4,5-tris{3-(N-tert-butoxycarbonyl)amino-1-propanoxy}benzoylamino]hexanoic acid
• CAS No.: 1031684-79-3
• Molecular Formula: C₃₇H₆₂N₄O₁₂
• Molecular Weight: 754.919

Synonyms:6-[3,4,5-tris{3-(N-tert-butoxycarbonyl)amino-1-propanoxy}benzoylamino]hexanoic acid

Chemical Property of 6-[3,4,5-tris{3-(N-tert-butoxycarbonyl)amino-1-propanoxy}benzoylamino]hexanoic acid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 6-[3,4,5-tris{3-(N-tert-butoxycarbonyl)amino-1-propanoxy}benzoylamino]hexanoic acid

There total 1 articles about 6-[3,4,5-tris{3-(N-tert-butoxycarbonyl)amino-1-propanoxy}benzoylamino]hexanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

6-[3,4,5-tris{3-(N-tert-butoxycarbonyl)amino-1-propanoxy}benzoylamino]hexanoic acid methyl ester (1031684-78-2) → 6-[3,4,5-tris{3-(N-tert-butoxycarbonyl)amino-1-propanoxy}benzoylamino]hexanoic acid (1031684-79-3)

Guidance literature:

With potassium hydroxide; water; In methanol; dichloromethane; Reflux;

DOI:10.1002/chem.200701634

Reference yield: 84.0%

N-S(trityl)-L-cysteinyl-L-valyl-L-isoleucyl-L-leucine t-butyl ester (1031684-73-7) + 6-[3,4,5-tris{3-(N-tert-butoxycarbonyl)amino-1-propanoxy}benzoylamino]hexanoic acid (1031684-79-3) → N-(5-{3,4,5-tris[3-N-(tert-butoxycarbonyl)amino-1-propanoxy]benzoylamine}pentanylcarbonyl)-S(trityl)-L-cysteinyl-L-valyl-L-isoleucyl-L-leucine t-butyl ester (1031684-81-7)

Guidance literature:

With (benzotriazole-1-yloxy)tris(pyrrolidino)phosphonium hexafluorophosphate; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide;

DOI:10.1002/chem.200701634

Reference yield: 67.0%

6-[3,4,5-tris{3-(N-tert-butoxycarbonyl)amino-1-propanoxy}benzoylamino]hexanoic acid (1031684-79-3) + N-S(trityl)-L-cysteinyl-L-valyl-L-isoleucyl-L-methionyl t-butyl ester (1259519-08-8) → 6-{3,4,5-tris[3-N-(t-butoxycarbonyl)amino-1-propanoxy]benzoylamino}hexanoyl-S(trityl)-L-cysteinyl-L-valyl-L-isoleucyl-L-methionine t-butyl ester (1259518-89-2)

Guidance literature:

With (benzotriazole-1-yloxy)tris(pyrrolidino)phosphonium hexafluorophosphate; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 0 - 20 ℃;

DOI:10.1021/jal086112

upstream raw materials:

6-[3,4,5-tris{3-(N-tert-butoxycarbonyl)amino-1-propanoxy}benzoylamino]hexanoic acid methyl ester

Downstream raw materials:

N-(5-{3,4,5-tris[3-N-(tert-butoxycarbonyl)amino-1-propanoxy]benzoylamine}pentanylcarbonyl)-S(trityl)-L-cysteinyl-L-valyl-L-isoleucyl-L-leucine t-butyl ester

6-{3,4,5-tris[3-N-(t-butoxycarbonyl)amino-1-propanoxy]benzoylamino}hexanoyl-S(trityl)-L-cysteinyl-L-valyl-L-isoleucyl-L-methionine t-butyl ester

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