((S)S,1R,2S)-(+)-N-methoxy-N-methyl-2-(p-toluenesulfinylamino)-cyclopent-3-enyl amide

Base Information

• Chemical Name: ((S)S,1R,2S)-(+)-N-methoxy-N-methyl-2-(p-toluenesulfinylamino)-cyclopent-3-enyl amide
• CAS No.: 1228389-06-7
• Molecular Formula: C₁₅H₂₀N₂O₃S
• Molecular Weight: 308.401

Synonyms:((S)S,1R,2S)-(+)-N-methoxy-N-methyl-2-(p-toluenesulfinylamino)-cyclopent-3-enyl amide

Chemical Property of ((S)S,1R,2S)-(+)-N-methoxy-N-methyl-2-(p-toluenesulfinylamino)-cyclopent-3-enyl amide

Chemical Property:

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Technology Process of ((S)S,1R,2S)-(+)-N-methoxy-N-methyl-2-(p-toluenesulfinylamino)-cyclopent-3-enyl amide

There total 1 articles about ((S)S,1R,2S)-(+)-N-methoxy-N-methyl-2-(p-toluenesulfinylamino)-cyclopent-3-enyl amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

C17H24N2O3S (1228389-03-4) → ((S)S,1R,2S)-(+)-N-methoxy-N-methyl-2-(p-toluenesulfinylamino)-cyclopent-3-enyl amide (1228389-06-7)

Guidance literature:

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In dichloromethane; at 20 ℃; Inert atmosphere;

DOI:10.1021/jo100680b

Reference yield: 84.0%

((S)S,1R,2S)-(+)-N-methoxy-N-methyl-2-(p-toluenesulfinylamino)-cyclopent-3-enyl amide (1228389-06-7) + methylmagnesium bromide (75-16-1) → 1-((S(S),1R,2S)-2-(p-toluenesulfinylamino)cyclopent-3-enyl)ethanone

Guidance literature:

((S)S,1R,2S)-(+)-N-methoxy-N-methyl-2-(p-toluenesulfinylamino)-cyclopent-3-enyl amide; methylmagnesium bromide; In tetrahydrofuran; at -15 ℃; for 2h; Inert atmosphere;

With ammonium chloride; In tetrahydrofuran; at 0 - 20 ℃; Saturated solution;

DOI:10.1021/jo100680b

upstream raw materials:

C₁₇H₂₄N₂O₃S

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