pentachlorophenyl 2,6-anhydro-3,4,5,7-tetra-O-benzoyl-D-glycero-D-gulo-heptonate

Base Information

Chemical Name:pentachlorophenyl 2,6-anhydro-3,4,5,7-tetra-O-benzoyl-D-glycero-D-gulo-heptonate
CAS No.:848034-61-7
Molecular Formula:C₄₁H₂₇Cl₅O₁₁
Molecular Weight:872.924
Hs Code.:

Synonyms:pentachlorophenyl 2,6-anhydro-3,4,5,7-tetra-O-benzoyl-D-glycero-D-gulo-heptonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of pentachlorophenyl 2,6-anhydro-3,4,5,7-tetra-O-benzoyl-D-glycero-D-gulo-heptonate

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Technology Process of pentachlorophenyl 2,6-anhydro-3,4,5,7-tetra-O-benzoyl-D-glycero-D-gulo-heptonate

There total 2 articles about pentachlorophenyl 2,6-anhydro-3,4,5,7-tetra-O-benzoyl-D-glycero-D-gulo-heptonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 848034-51-5
(2R,3R,4S,5R,6R)-3,4,5-tris(benzoyloxy)-6-((benzoyloxy)methyl)tetrahydro-2H-pyran-2-carboxylic acid

: 87-86-5,67471-28-7
Pentachlorophenol

: 848034-61-7
pentachlorophenyl 2,6-anhydro-3,4,5,7-tetra-O-benzoyl-D-glycero-D-gulo-heptonate

Guidance literature:: With dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃;
DOI:10.1016/j.tetasy.2004.11.064

Reference yield:

: 286369-06-0
2,6-anhydro-3,4,5,7-tetra-O-benzoyl-D-glycero-D-gulo-heptonamide

: 848034-61-7
pentachlorophenyl 2,6-anhydro-3,4,5,7-tetra-O-benzoyl-D-glycero-D-gulo-heptonate

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / nitrogen(IV) oxide / CH₂Cl₂ / 20 °C

2: 89 percent / 1,3-dicyclohexylcarbodiimide / CH₂Cl₂ / 20 °C

With Nitrogen dioxide; dicyclohexyl-carbodiimide; In dichloromethane;
DOI:10.1016/j.tetasy.2004.11.064