4-dibenzylamino-2,5-dimethylbenzaldehyde hydrochloride

Base Information

Chemical Name:4-dibenzylamino-2,5-dimethylbenzaldehyde hydrochloride
CAS No.:953394-05-3
Molecular Formula:C₂₃H₂₃NO*ClH
Molecular Weight:365.903
Hs Code.:

Synonyms:4-dibenzylamino-2,5-dimethylbenzaldehyde hydrochloride

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Chemical Property of 4-dibenzylamino-2,5-dimethylbenzaldehyde hydrochloride

Chemical Property:

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Technology Process of 4-dibenzylamino-2,5-dimethylbenzaldehyde hydrochloride

There total 2 articles about 4-dibenzylamino-2,5-dimethylbenzaldehyde hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 953394-05-3
4-dibenzylamino-2,5-dimethylbenzaldehyde hydrochloride

Guidance literature:: dibenzyl-(4-iodo-2,5-dimethylphenyl)amine; In toluene; for 0.25h;

With n-butyllithium; In hexane; toluene; at -20 - -10 ℃; for 0.25h;

N,N-dimethyl-formamide; With hydrogenchloride; more than 3 stages;

Reference yield:

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 953394-05-3
4-dibenzylamino-2,5-dimethylbenzaldehyde hydrochloride

: C₂₂H₂₃N*ClH

Guidance literature:: dibenzyl-(4-iodo-2,5-dimethylphenyl)amine; With n-butyllithium; In hexane; toluene; at -15 - -10 ℃; for 0.25h;

N,N-dimethyl-formamide; In hexane; toluene; at -20 - 0 ℃; for 1h;

With hydrogenchloride; In hexane; water; toluene; for 0.333333h;

Reference yield:

: 953394-05-3
4-dibenzylamino-2,5-dimethylbenzaldehyde hydrochloride

: 107-21-1
ethylene glycol

: 954136-51-7
dibenzyl-(4-[1,3]dioxolan-2-yl-2,5-dimethyl-phenyl)amine

Guidance literature:: 4-dibenzylamino-2,5-dimethylbenzaldehyde hydrochloride; ethylene glycol; With toluene-4-sulfonic acid; In toluene; at 60 - 80 ℃; for 20h;

With sodium hydrogencarbonate; In water; ethyl acetate;