2-((4,6-dimethoxy-2-pyrimidinyl)oxy)-3-methoxy-3,3-diphenylpropionitrile

Base Information

Chemical Name:2-((4,6-dimethoxy-2-pyrimidinyl)oxy)-3-methoxy-3,3-diphenylpropionitrile
CAS No.:178306-56-4
Molecular Formula:C₂₂H₂₁N₃O₄
Molecular Weight:391.426
Hs Code.:

Synonyms:2-((4,6-dimethoxy-2-pyrimidinyl)oxy)-3-methoxy-3,3-diphenylpropionitrile

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-((4,6-dimethoxy-2-pyrimidinyl)oxy)-3-methoxy-3,3-diphenylpropionitrile

Chemical Property:

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Technology Process of 2-((4,6-dimethoxy-2-pyrimidinyl)oxy)-3-methoxy-3,3-diphenylpropionitrile

There total 4 articles about 2-((4,6-dimethoxy-2-pyrimidinyl)oxy)-3-methoxy-3,3-diphenylpropionitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 178306-55-3
2-hydroxy-3-methoxy-3,3-diphenylpropionitrile

: 113583-35-0
4,6-dimethoxypyrimidin-2-yl methyl sulfone

: 178306-56-4
2-((4,6-dimethoxy-2-pyrimidinyl)oxy)-3-methoxy-3,3-diphenylpropionitrile

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 12h;

Reference yield:

: 178306-55-3
2-hydroxy-3-methoxy-3,3-diphenylpropionitrile

: 584-08-7
potassium carbonate

: 113583-35-0
4,6-dimethoxypyrimidin-2-yl methyl sulfone

: 178306-56-4
2-((4,6-dimethoxy-2-pyrimidinyl)oxy)-3-methoxy-3,3-diphenylpropionitrile

Guidance literature:: In N,N-dimethyl-formamide;

Reference yield:

: 119-61-9
benzophenone

: 178306-56-4
2-((4,6-dimethoxy-2-pyrimidinyl)oxy)-3-methoxy-3,3-diphenylpropionitrile

Guidance literature:: Multi-step reaction with 3 steps

1: sodium methylate / tetrahydrofuran / 2 h / -10 °C

2: boron trifluoride diethyl etherate / 0 - 20 °C

3: potassium carbonate / N,N-dimethyl-formamide / 12 h / 20 °C

With boron trifluoride diethyl etherate; sodium methylate; potassium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide;