trans-4-(1-amino-butyl)-4-(4-fluoro-phenyl)-cyclohexanol hydrochloride

Base Information

Chemical Name:trans-4-(1-amino-butyl)-4-(4-fluoro-phenyl)-cyclohexanol hydrochloride
CAS No.:1202007-07-5
Molecular Formula:C₁₆H₂₄FNO*ClH
Molecular Weight:301.832
Hs Code.:

Synonyms:trans-4-(1-amino-butyl)-4-(4-fluoro-phenyl)-cyclohexanol hydrochloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of trans-4-(1-amino-butyl)-4-(4-fluoro-phenyl)-cyclohexanol hydrochloride

Chemical Property:

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Technology Process of trans-4-(1-amino-butyl)-4-(4-fluoro-phenyl)-cyclohexanol hydrochloride

There total 8 articles about trans-4-(1-amino-butyl)-4-(4-fluoro-phenyl)-cyclohexanol hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1202007-05-3
trans-{1-[1-(4-fluoro-phenyl)-4-hydroxy-cyclohexyl]-butyl}-carbamic acid tert-butyl ester

: 1202007-07-5
trans-4-(1-amino-butyl)-4-(4-fluoro-phenyl)-cyclohexanol hydrochloride

Guidance literature:: With hydrogenchloride; In water; isopropyl alcohol;

Reference yield:

: 1202007-04-2
{1-[1-(4-fluoro-phenyl)-4-oxo-cyclohexyl]-butyl}-carbamic acid tert-butyl ester

: 1202007-07-5
trans-4-(1-amino-butyl)-4-(4-fluoro-phenyl)-cyclohexanol hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate / ethanol / -20 - 20 °C

2: hydrogenchloride / water; isopropyl alcohol

With hydrogenchloride; sodium tetrahydroborate; In ethanol; water; isopropyl alcohol;

Reference yield:

: 56326-95-5
methyl 5-cyano-5-(4-fluorophenyl)-2-oxocyclohexanecarboxylate

: 1202007-07-5
trans-4-(1-amino-butyl)-4-(4-fluoro-phenyl)-cyclohexanol hydrochloride

Guidance literature:: Multi-step reaction with 8 steps

1: hydrogenchloride / ethanol; water / 40 h / Reflux

2: toluene-4-sulfonic acid / toluene / 6 h / Heating

3: diethyl ether / Reflux

4: sodium tetrahydroborate / diethyl ether

5: triethylamine / dichloromethane / 20 °C

6: hydrogenchloride / water; acetone / 20 °C

7: sodium tetrahydroborate / ethanol / -20 - 20 °C

8: hydrogenchloride / water; isopropyl alcohol

With hydrogenchloride; sodium tetrahydroborate; toluene-4-sulfonic acid; triethylamine; In diethyl ether; ethanol; dichloromethane; water; isopropyl alcohol; acetone; toluene;