4-(3-carbonylbenzo[d][1,2]selenazole-2(3H))-phenylethyl-1-hydroxyl-methylenediphosphonic acid

Base Information

Chemical Name:4-(3-carbonylbenzo[d][1,2]selenazole-2(3H))-phenylethyl-1-hydroxyl-methylenediphosphonic acid
CAS No.:1374330-07-0
Molecular Formula:C₁₅H₁₅NO₈P₂S
Molecular Weight:431.3
Hs Code.:

Synonyms:4-(3-carbonylbenzo[d][1,2]selenazole-2(3H))-phenylethyl-1-hydroxyl-methylenediphosphonic acid

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Chemical Property of 4-(3-carbonylbenzo[d][1,2]selenazole-2(3H))-phenylethyl-1-hydroxyl-methylenediphosphonic acid

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Technology Process of 4-(3-carbonylbenzo[d][1,2]selenazole-2(3H))-phenylethyl-1-hydroxyl-methylenediphosphonic acid

There total 4 articles about 4-(3-carbonylbenzo[d][1,2]selenazole-2(3H))-phenylethyl-1-hydroxyl-methylenediphosphonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 93371-97-2
metile 4-(3-oxo-1,2-benzisotiazolin-2-il)acetato

: 1374330-07-0
4-(3-carbonylbenzo[d][1,2]selenazole-2(3H))-phenylethyl-1-hydroxyl-methylenediphosphonic acid

Guidance literature:: With phosphonic Acid; phosphorus trichloride; at 100 ℃; for 2h;

Reference yield:

: 118-92-3,159201-01-1,50816-84-7,80206-34-4,104809-47-4
anthranilic acid

: 1374330-07-0
4-(3-carbonylbenzo[d][1,2]selenazole-2(3H))-phenylethyl-1-hydroxyl-methylenediphosphonic acid

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium nitrite; hydrogenchloride / water / 0 - 5 °C

1.2: 5 h / 60 °C

2.1: thionyl chloride / 3 h / 80 °C

3.1: sodium hydrogencarbonate / water; diethyl ether / 6 h / 20 °C / Cooling with ice

4.1: phosphonic Acid; phosphorus trichloride / 2 h / 100 °C

With hydrogenchloride; phosphonic Acid; thionyl chloride; sodium hydrogencarbonate; sodium nitrite; phosphorus trichloride; In diethyl ether; water;

Reference yield:

: 119-80-2
2,2'-dithiobenzoic acid

: 1374330-07-0
4-(3-carbonylbenzo[d][1,2]selenazole-2(3H))-phenylethyl-1-hydroxyl-methylenediphosphonic acid

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride / 3 h / 80 °C

2: sodium hydrogencarbonate / water; diethyl ether / 6 h / 20 °C / Cooling with ice

3: phosphonic Acid; phosphorus trichloride / 2 h / 100 °C

With phosphonic Acid; thionyl chloride; sodium hydrogencarbonate; phosphorus trichloride; In diethyl ether; water;